Erigeside C

Base Information

• Chemical Name: Erigeside C
• CAS No.: 112667-09-1
• Molecular Formula: C₁₅H₂₀O₁₀
• Molecular Weight: 360.318
• Mol file: 112667-09-1.mol

Synonyms:ErigesideC; Syringic acid 1-O-b-D-glucose ester; Syringic acid b-glucopyranosyl ester

Chemical Property of Erigeside C

Chemical Property:

• Boiling Point: 618.5±55.0 °C(Predicted)
• PKA: 8.04±0.25(Predicted)
• PSA: 155.14000
• Density: 1.57±0.1 g/cm3(Predicted)
• LogP: -1.63390

Purity/Quality:

98%min ^*data from raw suppliers

Erigeside C ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Erigeside C

There total 6 articles about Erigeside C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Benzoyloxy-benzoic acid (4aR,6S,7R,8R,8aS)-7,8-dihydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yl ester → 3,5-dimethoxy-4-hydroxybenzoic acid-O-β-D-glucopyranoside (112667-09-1)

Guidance literature:

With hydrogen; acetic acid; palladium on activated charcoal; In ethanol; ethyl acetate; for 2h; Ambient temperature;

DOI:10.1016/0031-9422(88)80121-3

Reference yield:

4-(benzoyloxy)benzoyl chloride (58860-84-7) → 3,5-dimethoxy-4-hydroxybenzoic acid-O-β-D-glucopyranoside (112667-09-1)

Guidance literature:

Multi-step reaction with 2 steps

1: CHCl₃ / 90 h / Ambient temperature

2: H₂, HOAc / 10percent Pd/C / ethanol; ethyl acetate / 2 h / Ambient temperature

With hydrogen; acetic acid; palladium on activated charcoal; In ethanol; chloroform; ethyl acetate;

DOI:10.1016/0031-9422(88)80121-3

Reference yield:

4,6-benzylidene-α-D-glucose sodium → 3,5-dimethoxy-4-hydroxybenzoic acid-O-β-D-glucopyranoside (112667-09-1)

Guidance literature:

Multi-step reaction with 2 steps

1: CHCl₃ / 90 h / Ambient temperature

2: H₂, HOAc / 10percent Pd/C / ethanol; ethyl acetate / 2 h / Ambient temperature

With hydrogen; acetic acid; palladium on activated charcoal; In ethanol; chloroform; ethyl acetate;

DOI:10.1016/0031-9422(88)80121-3

upstream raw materials:

D-glucose

4-(benzoyloxy)benzoyl chloride

benzoyl chloride

3,5-dimethoxy-4-hydroxybenzoic acid

Refernces

• 1、 Klick, Silke,Herrmann, Karl. "GLUCOSIDES AND GLUCOSE ESTERS OF HYDROXYBENZOIC ACIDS IN PLANTS". . p. 2177 - 2180. Retrieved 2007/10/02.