N-(3-Aminopropyl)-N-dodecylpropane-1,3-diamine

Base Information

• Chemical Name: N-(3-Aminopropyl)-N-dodecylpropane-1,3-diamine
• CAS No.: 2372-82-9
• Molecular Formula: C18H41N3
• Molecular Weight: 299.544
• Hs Code.: 2921290000
• European Community (EC) Number: 219-145-8
• UNII: PCJ6308JUE
• DSSTox Substance ID: DTXSID3041243
• Nikkaji Number: J213.232J
• Wikidata: Q27286479
• RXCUI: 2384783
• Mol file: 2372-82-9.mol

Synonyms:bis(aminopropyl)laurylamine;N-(3-aminopropyl)-N-dodecylpropane-1,3-diamine

Chemical Property of N-(3-Aminopropyl)-N-dodecylpropane-1,3-diamine

Chemical Property:

• Appearance/Colour: Liquid
• Vapor Pressure: 3.63E-06mmHg at 25°C
• Refractive Index: 1.477
• Boiling Point: 386.1 °C at 760mmHg
• PKA: 10.46±0.10(Predicted)
• Flash Point: 184.5 °C
• PSA: 55.28000
• Density: 0.88 g/cm³
• LogP: 5.30750
• Solubility.: 560g/L in organic solvents at 20 ℃
• Water Solubility.: 190g/L at 20℃
• XLogP3: 4.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 17
• Exact Mass: 299.330048321
• Heavy Atom Count: 21
• Complexity: 177

Purity/Quality:

98%min ^*data from raw suppliers

N-?(3-?Aminopropyl)?-?n-?dodecylpropane-?1,?3-?diamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCN(CCCN)CCCN
• Description: N-(3-Aminopropyl)-n-dodecylpropane-1,3-diamine, also called N,N-bis(3-aminopropyl)dodecylamine and laurylamine dipropylenediamine, is dodecylamine substituted with 2 propylamine units. Laurylamine dipropylenediamine is a non-ionic surfactant, antimicrobial agent, preservative, emulsifying agent, dispersing agent, corrosion inhibitor and an anti-static agent used in hair products.
• Uses: N-(3-aminopropyl)-N-dodecylpropane-1,3-diamine is used as disinfectant for food processing industry, institutions, hospitals (surfaces and instruments).N-?(3-?Aminopropyl)?-?n-?dodecylpropane-?1,?3-?diamine is a reactant used in the synthesis of gluconamide derivatives as cationic surfactants with antimicrobial properties. Lonzabac(R) 12.30 is used as disinfectant for food processing industry, institutions, hospitals (surfaces and instruments)..

Technology Process of N-(3-Aminopropyl)-N-dodecylpropane-1,3-diamine

There total 5 articles about N-(3-Aminopropyl)-N-dodecylpropane-1,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-dodecyl-2,2'-iminodipropionitrile (1555-62-0) → N-(3-aminopropyl)-N-dodecyl-1,3-propanediamine (2372-82-9)

Guidance literature:

With ethanol; nickel; at 95 ℃; under 14710.2 Torr; Hydrogenation;

Reference yield:

n-Dodecylamine (124-22-1) → N-(3-aminopropyl)-N-dodecyl-1,3-propanediamine (2372-82-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / methanol / 16 h / 45 °C

2: NH₃; H₂ / Raney nickel / methanol / 24 h / 2585.81 Torr

With ammonia; hydrogen; nickel; In methanol;

DOI:10.1021/jo070245v

Reference yield:

concentrated acetic acid + n-Dodecylamine (124-22-1) + acrylonitrile (107-13-1,25014-41-9) → N-(3-aminopropyl)-N-dodecyl-1,3-propanediamine (2372-82-9)

Guidance literature:

In methanol; water;

upstream raw materials:

N-dodecyl-2,2'-iminodipropionitrile

n-Dodecylamine

acrylonitrile

1,4-dioxane

Refernces

• 1、 Denton, Travis T.,Joyce, Abigail S.,Kiely, Donald E.. "Preparation of N-alkylbis(3-aminopropyl)amines by the catalytic hydrogenation of N-alkylbis(cyanoethyl)amines". . p. 4997 - 5000. Retrieved 2008/02/05.
• 2、 -. "Bis-betaine-amine oxides, process for their preparation, and cleaning agents containing them". . . Retrieved 2008/06/13.