C₆₆H₁₁₃NO₁₃Si₂

Base Information

• Chemical Name: C₆₆H₁₁₃NO₁₃Si₂
• CAS No.: 186417-28-7
• Molecular Formula: C₆₆H₁₁₃NO₁₃Si₂
• Molecular Weight: 1184.79
• Mol file: 186417-28-7.mol

Synonyms:C₆₆H₁₁₃NO₁₃Si₂

Chemical Property of C₆₆H₁₁₃NO₁₃Si₂

Chemical Property:

Purity/Quality:

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Technology Process of C₆₆H₁₁₃NO₁₃Si₂

There total 34 articles about C₆₆H₁₁₃NO₁₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

t-butyldimethylsiyl triflate (69739-34-0) + C60H99NO13Si (151122-98-4) → C66H113NO13Si2 (186417-28-7)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃;

DOI:10.1021/ja963067o

Reference yield: 90.0%

C72H127NO13Si3 (164592-91-0) → C66H113NO13Si2 (186417-28-7)

Guidance literature:

With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 0 ℃; for 3h;

DOI:10.1021/ja963067o

Reference yield: 90.0%

C69H121NO13Si3 (186417-32-3) → C66H113NO13Si2 (186417-28-7)

Guidance literature:

With tetrabutyl ammonium fluoride; acetic acid; at 0 ℃; for 0.5h;

DOI:10.1021/ja963067o

upstream raw materials:

t-butyldimethylsiyl triflate

C₆₀H₉₉NO₁₃Si

C₇₂H₁₂₇NO₁₃Si₃

C₆₉H₁₂₁NO₁₃Si₃

Downstream raw materials:

C₇₂H₁₂₇NO₁₃Si₃

sirolimus

C₇₂H₁₂₇NO₁₃Si₃

C₆₉H₁₂₁NO₁₃Si₃

Refernces