Technology Process of 1-dodecyl-4-methoxy-benzene
There total 22 articles about 1-dodecyl-4-methoxy-benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; potassium tert-butylate; 1,3,5,7-tetramethyl-6-(2,4-dimethoxyphenyl)-2,4,8-trioxa-6-phosphaadamantane;
In
1,4-dioxane;
at 20 ℃;
for 26h;
DOI:10.1021/jo048875+
- Guidance literature:
-
1-bromo-4-methoxy-benzene;
With
tert.-butyl lithium;
In
tetrahydrofuran; n-heptane;
at -80 ℃;
for 2h;
Inert atmosphere;
1-Bromodocosane;
In
tetrahydrofuran; n-heptane;
at -80 - 20 ℃;
for 48h;
Inert atmosphere;
With
toluene-4-sulfonic acid;
In
ethanol;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1039/c9tc06456g
- Guidance literature:
-
With
[2,2]bipyridinyl; vitamin B12; manganese; chloro-trimethyl-silane; potassium iodide; nickel dibromide;
In
N,N-dimethyl-formamide;
at 30 ℃;
for 30h;
Reagent/catalyst;
Schlenk technique;
Inert atmosphere;
DOI:10.1039/c7cc01932g
