4-Decylaniline

Base Information

• Chemical Name: 4-Decylaniline
• CAS No.: 37529-30-9
• Molecular Formula: C16H27N
• Molecular Weight: 233.397
• Hs Code.: 29214990
• European Community (EC) Number: 253-546-9
• UNII: 25X74W976X
• DSSTox Substance ID: DTXSID9022287
• Nikkaji Number: J150.044I
• Wikidata: Q27254007
• Mol file: 37529-30-9.mol

Synonyms:4-Decylaniline;37529-30-9;4-n-Decylaniline;Benzenamine, 4-decyl-;p-Decylaniline;p-n-Decylaniline;EINECS 253-546-9;UNII-25X74W976X;MFCD00007918;25X74W976X;4-decylphenylamine;4-Decylaniline, 97%;4-DECYLBENZENAMINE;SCHEMBL111357;DTXSID9022287;AKOS005254412;DS-13883;LS-184977;AM20050230;CS-0152248;D2731;FT-0639382;A823730;Q27254007

Chemical Property of 4-Decylaniline

Chemical Property:

• Vapor Pressure: 1.69E-05mmHg at 25°C
• Melting Point: 25 °C(lit.)
• Refractive Index: 1.5100
• Boiling Point: 364.4 °C at 760 mmHg
• PKA: 4.96±0.10(Predicted)
• Flash Point: 150 °C
• PSA: 26.02000
• Density: 0.909 g/cm³
• LogP: 5.53320
• Sensitive.: Air Sensitive
• Water Solubility.: Insoluble in water.
• XLogP3: 6.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 9
• Exact Mass: 233.214349865
• Heavy Atom Count: 17
• Complexity: 159

Purity/Quality:

98%min ^*data from raw suppliers

4-Decylaniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCC1=CC=C(C=C1)N
• Uses: It is used to synthesize p,p'-Di-n-decyl-azobenzol could be obtained by the reactant of 4-Decylaniline, and the reagents of O2, CuCl, pyridine.

Technology Process of 4-Decylaniline

There total 14 articles about 4-Decylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

→ 4-n-decylaniline (37529-30-9)

Guidance literature:

With platinum(IV) oxide; hydrogen; In ethanol; for 2h;

Reference yield: 83.0%

4-(dec-1-yn-1-yl)aniline (1423616-68-5) → 4-n-decylaniline (37529-30-9)

Guidance literature:

With platinum(IV) oxide; hydrogen; In methanol; at 20 ℃; for 24h; under 760.051 Torr;

DOI:10.1246/cl.2012.1566

Reference yield: 49.1%

1-Decanol (112-30-1) + aniline (62-53-3) → 4-n-decylaniline (37529-30-9)

Guidance literature:

With zinc(II) chloride; at 255 - 258 ℃; for 21h;

upstream raw materials:

4'-aminodecanoylphenone

1-Decanol

aniline hydrochloride

aniline

Downstream raw materials:

N-(4-decylphenyl)acetamide

1-decyl-4-iodobenzene

[2-benzyloxy-1-(4-decyl-phenylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester

Refernces

• 1、 Takeuchi, Makoto,Kurahashi, Takuya,Matsubara, Seijiro. "Nickel-catalyzed decarbonylative polymerization of 5-alkynylphthalimides: A new methodology for the preparation of polyheterocycles". . p. 1566 - 1568. Retrieved 2013/01/15.
• 2、 -. "Therapeutic agent for osteoporosis and diazepine compound". . . Retrieved 2008/06/13.