DL-MUSCONE

Base Information

• Chemical Name: DL-MUSCONE
• CAS No.: 956-82-1
• Molecular Formula: C16H30O
• Molecular Weight: 238.414
• Hs Code.: 2914299000
• Mol file: 956-82-1.mol

Synonyms:3-Methylcyclopentadecanone; 3-Methyl-1-cyclopentadecanone; 5-Methyl-1-cyclopentadecanone; AI3-38746; Cyclopentadecanone, 3-methyl-; FEMA No. 3434; HSDB 1219; Methylexaltone; Moschus ketone; 3-Methylcyclopentadecan-1-one; 3-Methylcyclopentadecanone, dl-; 4-tert-butyl-2,6-dimethyl-3,5-dinitroacetophenone; 4'-tert-butyl-2',6'-dimethyl-3',5'-dinitroacetophenone; 1-(4-tert-butyl-2,6-dimethyl-3,5-dinitrophenyl)ethanone; Musk Ketone

Chemical Property of DL-MUSCONE

Chemical Property:

• Vapor Pressure: 0.000176mmHg at 25°C
• Boiling Point: 329.5°C at 760 mmHg
• Flash Point: 145.3°C
• PSA: 17.07000
• Density: 0.843g/cm³
• LogP: 5.27650

Purity/Quality:

99% ^*data from raw suppliers

DL-MUSCONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Description: 3-Methyl-1-cyclopentadecanone has a soft, sweet, tenacious musky odor. May be prepared by the condensation of dodecamethyl-ene-a,α-dimethylketone hexadecane.

Technology Process of DL-MUSCONE

There total 215 articles about DL-MUSCONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-methylcyclopentadecenone (22442-01-9) → 3-methylcyclopentadecanone (956-82-1,22460-48-6)

Guidance literature:

With hydrogen; In ethanol; at 20 ℃; for 0.5h; under 760.051 Torr; chemoselective reaction;

DOI:10.1039/c1gc15217c

Reference yield: 95.32%

C24H39N → 3-methylcyclopentadecanone (956-82-1,22460-48-6)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 80 ℃; for 2h;

Reference yield: 94.0%

(Z)-3-methylcyclopentadec-3-en-1-one (22442-02-0,58643-72-4,58643-73-5) → 3-methylcyclopentadecanone (956-82-1,22460-48-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In cyclohexane; for 16h; Ambient temperature;

DOI:10.1002/hlca.19900730416

upstream raw materials:

3-methylhexadecanedioic acid

(4E,8E)-14-Methyl-16-oxa-bicyclo[10.3.1]hexadeca-4,8,13-triene

14-methyl-16-oxabicyclo[10.3.1]hexadecane

14-methylbicyclo<10.3.0>pentadec-1(12)-en-13-one

Downstream raw materials:

methylcyclopentadecane

succinic acid

1,12-dodecanedioic acid

(R)-3-methyl-1-cyclopentadecanone

Refernces

• 1、 -. "Preparation method of musk ketone". Paragraph 0059; 0069-0071. . Retrieved 2020/12/30.
• 2、 -. "Continuous preparation method of DL-muscone". Paragraph 0046; 0048; 0050; 0051; 0053; 0054; 0055; 0056. . Retrieved 2018/07/15.