AKOS BBS-00005529

Base Information

• Chemical Name: AKOS BBS-00005529
• CAS No.: 39033-45-9
• Molecular Formula: C8H5Cl2NO
• Molecular Weight: 202.04
• Hs Code.: 2933990090
• Mol file: 39033-45-9.mol

Synonyms:AKOS BBS-00005529;ASISCHEM C58379;3,3-Dichloro-1,3-dihydro-2H-indol-2-one;3,3-Dichloro-1,3-dihydro-indol-2-one;3,3-dichloro-1H-indol-2-one;3,3-dichloro-2-indolinone;3,3-dichloroindolin-2-one;3,3-dichlorooxindole

Chemical Property of AKOS BBS-00005529

Chemical Property:

• Boiling Point: 334.8±42.0 °C(Predicted)
• PKA: 10.82±0.40(Predicted)
• PSA: 29.10000
• Density: 1.52±0.1 g/cm3(Predicted)
• LogP: 2.40710

Purity/Quality:

98%min ^*data from raw suppliers

3,3-dichloro-1,3-dihydro-2H-indol-2-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of AKOS BBS-00005529

There total 1 articles about AKOS BBS-00005529 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

indole (120-72-9) → 3,3-dichloro-2,3-dihydro-1H-indol-2-one (39033-45-9) + indole-2,3-dione (91-56-5,1186480-61-4,84788-92-1)

Guidance literature:

With C₁₂H₁₁Cl₃N₃V; In dichloromethane; at 20 ℃; for 1095.75h;

DOI:10.1002/ejic.201200148

Reference yield:

3,3-dichloro-2,3-dihydro-1H-indol-2-one (39033-45-9) + ortho-cresol (95-48-7,77504-84-8) → 3,3-bis(4-hydroxy-3-methylphenyl)-1H-indol-2-one (47465-97-4)

Guidance literature:

Reference yield:

3,3-dichloro-2,3-dihydro-1H-indol-2-one (39033-45-9) + sulfuric acid (7664-93-9) → indole-2,3-dione (91-56-5,1186480-61-4,84788-92-1)

Guidance literature:

at 60 ℃;

upstream raw materials:

indole

Downstream raw materials:

3,3-bis(4-hydroxy-3-methylphenyl)-1H-indol-2-one

Bisatin

3,3-diphenyl-1,3-dihydro-indol-2-one

oxyphenisatine

Refernces