o-(2-Methoxyethyl)phenol

Base Information

• Chemical Name: o-(2-Methoxyethyl)phenol
• CAS No.: 330976-39-1
• Molecular Formula: C₉H₁₂O₂
• Molecular Weight: 152.193
• Mol file: 330976-39-1.mol

Synonyms:2-(2-Methoxyethyl)phenol;o-(2-Methoxyethyl)phenol

Chemical Property of o-(2-Methoxyethyl)phenol

Chemical Property:

• PSA: 29.46000
• LogP: 1.58110
• Storage Temp.: Refrigerator
• Solubility.: Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

99% ^*data from raw suppliers

2-(2-Methoxyethyl)phenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: o-(2-Methoxyethyl)phenol is used as a stabilizer in the preparation of polysiloxane based coating compounds with good stability. 2-(2-Methoxyethyl)phenol is used as a stabilizer in the preparation of polysiloxane based coating compounds with good stability.

Technology Process of o-(2-Methoxyethyl)phenol

There total 4 articles about o-(2-Methoxyethyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2-(2-methoxyethenyl)phenol (1260168-27-1,397864-03-8) → 2-hydroxyphenethyl methyl ether (330976-39-1)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In methanol; at 20 ℃; for 2h; Reagent/catalyst; Solvent;

Reference yield: 82.0%

2-(o-cyanomethyl)phenethyl methyl ether → 2-hydroxyphenethyl methyl ether (330976-39-1)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethanol;

Reference yield:

salicylaldehyde (90-02-8) → 2-hydroxyphenethyl methyl ether (330976-39-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C

1.2: 4 h / 20 °C

2.1: 5%-palladium/activated carbon; hydrogen / methanol / 2 h / 20 °C

With 5%-palladium/activated carbon; potassium tert-butylate; hydrogen; In tetrahydrofuran; methanol;

upstream raw materials:

salicylaldehyde

2-(2-methoxyethenyl)phenol

Refernces

• 1、 -. "HYDROFORMYLATION PROCESS UTILIZING MULTIDENTATE PHOSPHITE LIGANDS". Page/Page column 26. . Retrieved 2010/02/10.