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Cas Database |
| Name |
1-Bromo-4-phenylbutane |
EINECS | N/A |
| CAS No. | 13633-25-5 | Density | 1.265 g/cm3 |
| PSA | 0.00000 | LogP | 3.40420 |
| Solubility | Slightly soluble in water. | Melting Point |
52 °C |
| Formula | C10H13Br | Boiling Point | 265.2 °C at 760 mmHg |
| Molecular Weight | 213.117 | Flash Point | 142.5 °C |
| Transport Information | N/A | Appearance | cream |
| Safety | 26-36 | Risk Codes | 36/37/38 |
| Molecular Structure |
|
Hazard Symbols |
 Xi
|
| Synonyms |
(4-Bromobutyl)benzene;1-Phenyl-4-bromobutane;4-Bromo-1-phenylbutane;4-Phenyl-1-bromobutane;4-Phenylbutyl bromide;NSC 89816; |
Article Data | 71 |
1-Bromo-4-phenylbutane Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With triphenylphosphine In dichloromethane; hexane-diethyl ether | 100% |
- 3360-41-6
4-phenyl-butan-1-ol
- 13633-25-5
1-Bromo-4-phenylbutane
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen bromide for 12h; Reagent/catalyst; Irradiation; Reflux; | 99.6% |
| With allyl bromide; 1,1'-carbonyldiimidazole In acetonitrile for 1h; Heating; | 98% |
| With carbon tetrabromide; triphenylphosphine In dichloromethane at 25℃; | 95% |
- 1229444-44-3
N-methyl-N-[4-(diphenylphosphino)benzyl]pyrrolidinium bromide
- 3360-41-6
4-phenyl-butan-1-ol
A
- 1229444-42-1
Br(1-)*C24H27NOP(1+)
B
- 13633-25-5
1-Bromo-4-phenylbutane
Conditions
| Conditions | Yield |
|---|---|
| With carbon tetrabromide In 1,2-dichloro-ethane at 40℃; for 2h; | A n/a B 97% |
- 1821-12-1
4-Phenylbutyric acid
- 13633-25-5
1-Bromo-4-phenylbutane
Conditions
| Conditions | Yield |
|---|---|
| With trimethylsilyl bromide; 1,1,3,3-Tetramethyldisiloxane; indium tribromide In chloroform at 60℃; for 4h; Sealed tube; Inert atmosphere; | 97% |
| With indium(III) bromide; 1,1,3,3-Tetramethyldisiloxane; trimethylsilyl cyanide In chloroform at 60℃; Inert atmosphere; | |
| Multi-step reaction with 2 steps 1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere 2: triphenylphosphine; carbon tetrabromide / acetonitrile / 3 h / 20 °C / Inert atmosphere View Scheme | |
| Multi-step reaction with 2 steps 1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 20 °C 2: triphenylphosphine; carbon tetrabromide / acetonitrile / 3 h / 20 °C View Scheme |
- 5558-00-9, 7515-41-5, 73611-78-6
(4-bromo-1-buten-1-yl)benzene
- 13633-25-5
1-Bromo-4-phenylbutane
Conditions
| Conditions | Yield |
|---|---|
| With palladium 10% on activated carbon; hydrogen In ethanol; water under 225.023 Torr; for 5h; | 93% |
- 1229444-43-2
4-(diphenylphosphino)-benzyltrimethylammonium bromide
- 3360-41-6
4-phenyl-butan-1-ol
A
- 1268610-56-5
Br(1-)*C22H25NOP(1+)
B
- 13633-25-5
1-Bromo-4-phenylbutane
Conditions
| Conditions | Yield |
|---|---|
| With carbon tetrabromide In 1,2-dichloro-ethane at 60℃; for 2h; | A n/a B 91% |
Conditions
| Conditions | Yield |
|---|---|
| at 5℃; for 2h; Temperature; | 85.8% |
Conditions
| Conditions | Yield |
|---|---|
| With copper(I) bromide; lithium bromide In tetrahydrofuran at 50 - 55℃; for 1h; | 85% |
- 369-57-3
benzenediazonium tetrafluoroborate
- 142172-51-8
4-bromo-1-butylboronic acid catechol ester
- 13633-25-5
1-Bromo-4-phenylbutane
Conditions
| Conditions | Yield |
|---|---|
| With 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride; palladium diacetate In tetrahydrofuran at 20℃; for 4.5h; Sizuki-Miyaura cross coupling; | 61% |
- 3360-41-6
4-phenyl-butan-1-ol
- 603-35-0
triphenylphosphine
A
- 13633-25-5
1-Bromo-4-phenylbutane
B
- 791-28-6
Triphenylphosphine oxide
Conditions
| Conditions | Yield |
|---|---|
| With carbon tetrabromide In 1,2-dichloro-ethane | A 53% B n/a |
1-Bromo-4-phenylbutane Chemical Properties
Product Name:1-Bromo-4-phenylbutane
CAS No:13633-25-5
Synonyms:RARECHEM AH CK 0044;1-BROMO-4-PHENYLBUTANE;(4-BROMOBUTYL)BENZENE;4-PHENYLBUTYL BROMIDE;4-PHENYL 1-BUTYL BROMIDE;4-Bromo-1-phenyl butane;1-BROMO-4-PHENYLBUTANE 99%;1-BROMO-4-PHENYL-BUTANE >97%
Molecular Formula:C10H13Br
Formula Weight:213.11
Density:1.214
Boiling Point:131-133°C/12mm
Flash Point:131-133°C/12mm
Molecular Structure:
CAS No:13633-25-5
Synonyms:RARECHEM AH CK 0044;1-BROMO-4-PHENYLBUTANE;(4-BROMOBUTYL)BENZENE;4-PHENYLBUTYL BROMIDE;4-PHENYL 1-BUTYL BROMIDE;4-Bromo-1-phenyl butane;1-BROMO-4-PHENYLBUTANE 99%;1-BROMO-4-PHENYL-BUTANE >97%
Molecular Formula:C10H13Br
Formula Weight:213.11
Density:1.214
Boiling Point:131-133°C/12mm
Flash Point:131-133°C/12mm
Molecular Structure:
1-Bromo-4-phenylbutane Safety Profile
Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 26-36
Hazard Note Irritant
Risk Statements 36/37/38
Safety Statements 26-36
Hazard Note Irritant
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1-Bromo-4-phenylbutane
