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1-TETRADECANOL
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Name

1-TETRADECANOL

 EINECS 204-000-3
CAS No. 112-72-1 Density 0.833 g/cm3
PSA 20.23000 LogP 4.67980
Solubility insoluble in water Melting Point 35-39 °C(lit.)
Formula C14H30O Boiling Point 263.2 °C at 760 mmHg
Molecular Weight 214.392 Flash Point 125.9 °C
Transport Information N/A Appearance white low melting solid or flakes
Safety 24/25 Risk Codes 38
Molecular Structure Molecular Structure of 112-72-1 (1-Tetradecanol) Hazard Symbols IrritantXi
Synonyms

Tetradecyl alcohol;n-Tetradecan-1-ol;n-Tetradecanol;n-Tetradecyl alcohol;Tetradecanol;Tetradecanol(7CI);1-Hydroxytetradecane;1-Tetradecyl alcohol;Adol 18;Alfol 14;Conol1495;Hinol 14SS;Kalcohl 40;Kalcohl 4098;Kalcol 4098;Lanette 14;Lanette K;Lanette Wax KS;Lorol C 14;Loxanol V;Myristic alcohol;Myristyl alcohol;NSC8549;Nacol 14-95;

Article Data 102

1-TETRADECANOL Synthetic route

124-10-7

methyl myristoate

112-72-1

1-Tetradecanol

Conditions
ConditionsYield
With C32H36ClNO2P2Ru; potassium tert-butylate; hydrogen In neat (no solvent) at 120℃; under 38002.6 Torr; for 20h; Autoclave; Green chemistry;99%
With [RuCl2(2-(diphenylphosphino)-N-((6-((diphenylphosphino)methyl)pyridin-2-yl)methyl)ethan-1-amine)]; potassium tert-butylate; hydrogen In tetrahydrofuran at 80℃; under 38002.6 Torr; for 5h; Catalytic behavior; Autoclave;97%
Stage #1: methyl myristoate With phenylsilane; fac-[Mn-(xantphos)(CO)3Br] at 120℃; for 12h; Inert atmosphere;
Stage #2: With water; sodium hydroxide In methanol at 20℃; Inert atmosphere;		96%

Tetradecyloxymethyl-benzene

112-72-1

1-Tetradecanol

Conditions
ConditionsYield
With 18-crown-6 ether; tert-butylamine; tert-butyl alcohol; potassium In tetrahydrofuran at 20℃; for 2h;98%
144708-82-7

1-Methoxymethoxy-tetradecane

112-72-1

1-Tetradecanol

Conditions
ConditionsYield
With methanol; DOWEX-50W-X2 for 30h; Heating;96%
108-88-3

toluene

Tetradecyloxymethyl-benzene

A

112-72-1

1-Tetradecanol

B

620-47-3

1-methyl-3-(phenylmethyl)-benzene

C

620-83-7

1-methyl-4-(phenylmethyl)benzene

D

713-36-0

2-benzyltoluene

Conditions
ConditionsYield
With boron trifluoride diethyl etherate at 120℃; for 2h;A 96%
B n/a
C n/a
D n/a
...Expand
77774-34-6

tetradecyl tert-butyldimethylsilyl ether

112-72-1

1-Tetradecanol

Conditions
ConditionsYield
With toluene-4-sulfonic acid In methanol; dichloromethane at 20 - 25℃; for 0.333333h; Flow reactor;96%
544-63-8

n-tetradecanoic acid

112-72-1

1-Tetradecanol

Conditions
ConditionsYield
With zirconium(IV) borohydride In tetrahydrofuran at 25℃; for 1h; Reduction;95%
With sodium tetrahydroborate; benzene-1,2-diol; trifluoroacetic acid In tetrahydrofuran at 25℃; for 4h;91%
With hydrogen In neat (no solvent) at 160℃; under 37503.8 Torr; for 24h;88%
124-06-1

Ethyl myristate

112-72-1

1-Tetradecanol

Conditions
ConditionsYield
With C30H34Cl2N2P2Ru; potassium methanolate; hydrogen In tetrahydrofuran at 100℃; under 38002.6 - 76005.1 Torr; for 15h; Glovebox; Autoclave;94%
With kieselguhr; copper at 350℃; under 73550.8 - 147102 Torr; Hydrogenation;
With lithium aluminium tetrahydride
146404-39-9

C21H38N2O2S

112-72-1

1-Tetradecanol

Conditions
ConditionsYield
With potassium hydroxide; ethanol; oxygen Heating;91%
14980-92-8

ethyl 2-bromomyristate

112-72-1

1-Tetradecanol

Conditions
ConditionsYield
With sodium tetrahydroborate at 65℃; for 24h;90%

4,4,5,5-tetramethyl-2-(tetradecyloxy)-1,3,2-dioxaborolane

112-72-1

1-Tetradecanol

Conditions
ConditionsYield
With water; silica gel In methanol at 60℃; Inert atmosphere;89%

1-TETRADECANOL Chemical Properties

Product Name: 1-Tetradecanol
Synonyms: Dytol R-52;dytolr-52;Dehydag wax 14;Emery 3334;Epal 14 ;Alfol 14;alfol14;Cachalot M-43 NF;
The Molecular formula of 1-TETRADECANOL(112-72-1): C14H30O
The Molecular Weight of 1-TETRADECANOL(112-72-1): 214.39
Molecular Structure : 
EINECS: 204-000-3
Melting point: 35-39 °C(lit.)
Boiling point: 289 °C(lit.)
Flash point: >230 °F
density: 0.823 g/mL at 25 °C(lit.)
vapor density: 7.4 (vs air)
storage temp.:-20°C
Water Solubility: insoluble

1-TETRADECANOL Uses

1-TETRADECANOL(112-72-1) is  used in organic synthesis and surfactant materials.

1-TETRADECANOL Toxicity Data With Reference

1.   

skn-hmn 75 mg/3D-I MOD

   85DKA8    Cutaneous Toxicity Drill, V.A. andP. Lazar, eds.,New York, NY.: Academic Press,1977,127.

1-TETRADECANOL Consensus Reports

Reported in EPA TSCA Inventory.

1-TETRADECANOL Safety Profile

Questionable carcinogen with experimental tumorigenic data. A human skin irritant. Combustible when exposed to heat or flame; can react with oxidizing materials. To fight fire, use CO2, dry chemical. When heated to decomposition it emits acrid smoke and irritating fumes. See also ALCOHOL, DENATURED; ALCOHOLS, C6-12; ALCOHOLS, C9-11; ALCOHOLS, C12-13, ETHOXYLATED; ALCOHOLS, C12-15, ETHOXYLATED; ALCOHOLS, C12-16, ETHOXYLATED; ALCOHOLS, C14-15, ETHOXYLATED; ALCOHOLS, C16-18, ETHOXYLATED; ALCOHOLS, C8-10, ETHOXYLATED PROPOXYLATED; ALCOHOLS, C12-15, ETHOXYLATED PROPOXYLATED; ALCOHOLS, N.O.S. and TETRADECANOL, mixed isomers.
The Hazard Codes of 1-TETRADECANOL(112-72-1):  Xi
The Risk Statements information of 1-TETRADECANOL(112-72-1):
38:  Irritating to the skin 
The Safety Statements information of 1-TETRADECANOL(112-72-1):
24/25:  Avoid contact with skin and eyes
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