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Name |
2,6-Dimethyl-4-hydroxypyridine |
EINECS | 237-089-2 |
CAS No. | 13603-44-6 | Density | 1.013 g/cm3 |
PSA | 33.12000 | LogP | 1.40400 |
Solubility | N/A | Melting Point |
230-232 °C |
Formula | C7H9NO | Boiling Point | 205.4 °C at 760 mm |
Molecular Weight | 123.155 | Flash Point | 93.1 °C |
Transport Information | N/A | Appearance | yellow to brown cryst |
Safety | 26-36 | Risk Codes | 36/37/38 |
Molecular Structure | Hazard Symbols | Xi | |
Synonyms |
2,6-Dimethyl-4-pyridinol;4-Hydroxy-2,6-dimethylpyridine;4-Hydroxy-2,6-lutidine;NSC 111932; |
Article Data | 24 |
Dehydracetic acid
2,6-dimethylpyridin-4-ol
Conditions | Yield |
---|---|
With ammonia In water at 120℃; for 0.333333h; Microwave irradiation; | 100% |
With ammonia In water at 120℃; for 0.333333h; Microwave irradiation; | 100% |
With ammonia In water at 120℃; for 0.333333h; microwave irradiation; | 100% |
4-bromo-2,6-dimethylpyridine
2,6-dimethylpyridin-4-ol
Conditions | Yield |
---|---|
With syn-benzaldehyde oxime; N1,N2-bis(thiophen-2-ylmethyl)oxalamide; caesium carbonate; copper(l) chloride In dimethyl sulfoxide at 80℃; for 20h; Reagent/catalyst; Temperature; Glovebox; Schlenk technique; Sealed tube; Inert atmosphere; | 50% |
2,6-dimethylpyrone
2,6-dimethylpyridin-4-ol
Conditions | Yield |
---|---|
With ammonium hydroxide at 100℃; | |
With ammonia at 25℃; | |
With ammonium hydroxide |
4-chloro-2,6-lutidine
2,6-dimethylpyridin-4-ol
Conditions | Yield |
---|---|
With sodium acetate; acetic acid at 200℃; Erhitzen des Reaktionsprodukts mit wss.Salzsaeure; |
4-amino-2,6-lutidine
2,6-dimethylpyridin-4-ol
Conditions | Yield |
---|---|
With sulfuric acid; water; sodium nitrite |
ethyl 4-chloro-2,6-dimethylnicotinate
2,6-dimethylpyridin-4-ol
Conditions | Yield |
---|---|
With hydrogenchloride at 150℃; |
trifluoromethylsulfonic anhydride
2,6-dimethylpyridin-4-ol
trifluoromethanesulfonic acid 2,6-dimethylpyridin-4-yl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 2.08333h; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 2.08333h; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 2.08333h; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 2.08333h; | 100% |
Stage #1: 2,6-dimethylpyridin-4-ol With triethylamine In dichloromethane at 0℃; for 0.166667h; Stage #2: trifluoromethylsulfonic anhydride; dmap In dichloromethane at 20℃; for 6h; | 79% |
2,6-dimethylpyridin-4-ol
Conditions | Yield |
---|---|
With bromine; tert-butylamine In methanol; dichloromethane at 5 - 20℃; for 2.66667h; Temperature; Reagent/catalyst; | 96% |
With bromine; tert-butylamine In methanol; dichloromethane at 5 - 20℃; for 2.66667h; | 96% |
With bromine; tert-butylamine In methanol; dichloromethane at 5 - 20℃; for 2.66667h; Reagent/catalyst; Temperature; | 96% |
With bromine; tert-butylamine In methanol; dichloromethane at 5 - 20℃; for 2.66667h; Concentration; Reagent/catalyst; Temperature; | 96% |
With bromine; tert-butylamine In methanol; dichloromethane at 5 - 20℃; for 2.66667h; Concentration; Reagent/catalyst; Temperature; | 96% |
2,6-dimethylpyridin-4-ol
Conditions | Yield |
---|---|
With bromine; tert-butylamine In methanol; dichloromethane at 20℃; for 2.66667h; | 96% |
With diisobutylamine; bromine In methanol; dichloromethane at 5 - 20℃; for 2.66667h; Reagent/catalyst; | 96% |
With bromine; tert-butylamine In methanol; dichloromethane at 5 - 20℃; for 2.66667h; | 96% |
2,6-dimethylpyridin-4-ol
3,5-dibromo-2,6-dimethylpyridin-4-ol
Conditions | Yield |
---|---|
With bromine; tert-butylamine In methanol; dichloromethane at 5 - 20℃; for 2.66667h; Temperature; | 96% |
With 4-methyl-morpholine; bromine In methanol; dichloromethane at 20℃; for 2h; | 88% |
With 4-methyl-morpholine; bromine In methanol; dichloromethane at 20℃; for 2h; Reagent/catalyst; Temperature; Cooling with ice; | 88% |