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2,6-Dimethylaniline
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Name

2,6-Dimethylaniline

 EINECS 201-758-7
CAS No. 87-62-7 Density 0.975 g/cm3
PSA 26.02000 LogP 2.46680
Solubility water: 7.5 g/L (20 °C) Melting Point 10-12 °C(lit.)
Formula C8H11N Boiling Point 217.9 °C at 760 mmHg
Molecular Weight 121.182 Flash Point 91.1 °C
Transport Information UN 1711 6.1/PG 2 Appearance colorless to reddish yellow liquid
Safety 23-25-36/37-61 Risk Codes 20/21/22-37/38-40-51/53
Molecular Structure Molecular Structure of 87-62-7 (2,6-Dimethylaniline) Hazard Symbols HarmfulXn,DangerousN,ToxicT
Synonyms

2,6-Xylidine(8CI);1-Amino-2,6-dimethylbenzene;2,6-Dimethylbenzenamine;2,6-Dimethylphenylamine;2,6-Xylylamine;2-Amino-1,3-dimethylbenzene;2-Amino-1,3-xylene;2-Amino-m-xylene;NSC 7098;o-Xylidine;2,6 Xylidine;

Article Data 192

2,6-Dimethylaniline Synthetic route

81-20-9

2,6-dimethylnitrobenzene

87-62-7

2,6-dimethylaniline

Conditions
ConditionsYield
With potassium fluoride; polymethylhydrosiloxane; palladium diacetate In tetrahydrofuran; water at 20℃; for 3h;100%
With potassium fluoride; polymethylhydrosiloxane; palladium diacetate In tetrahydrofuran at 20℃; for 0.5h;100%
With palladium 10% on activated carbon; hydrogen In methanol at 20℃; for 10h;100%
26334-20-3

2,6-dimethylphenylazide

87-62-7

2,6-dimethylaniline

Conditions
ConditionsYield
With sodium hydrogen telluride In diethyl ether; ethanol for 0.25h; Ambient temperature;100%
With aluminium(III) iodide In benzene for 0.166667h; Reduction; Heating;90%
With diphosphorus tetraiodide In benzene for 11h; Heating;40%
767-71-5

N-methyl-2,6-dimethylaniline

87-62-7

2,6-dimethylaniline

Conditions
ConditionsYield
With dichloro(dimethylglyoxime)(dimethylglyoximato)cobalt(III); (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; triethylamine In acetonitrile at -78℃; for 24h; Reagent/catalyst; Sealed tube; Inert atmosphere; Irradiation;100%
3095-48-5

4-amino-3,5-dimethyl-benzoic acid methyl ester

87-62-7

2,6-dimethylaniline

Conditions
ConditionsYield
With sodium hydroxide In water at 60 - 130℃; under 4560.31 Torr; for 3.5h; Temperature;99.1%

2-(2,6-dimethylphenyl)-4,5,6,7-tetrafluoroisoindoline-1,3-dione

87-62-7

2,6-dimethylaniline

Conditions
ConditionsYield
With ethylenediamine In ethanol at 65℃; for 14h;99%
6781-98-2

2,6-dimethyl-1-chlorobenzene

87-62-7

2,6-dimethylaniline

Conditions
ConditionsYield
With 2-((dicyclohexylphosphino)methyl)-1,3-bis(2,6-diisopropylphenyl)-4,5-dimethyl-1H-imidazol-3-ium iodide; ammonia; palladium diacetate; sodium t-butanolate In 1,4-dioxane at 120℃; under 7500.75 Torr; for 24h; Autoclave; Inert atmosphere;98%
With C28H30Cl5N3Pd; ammonia; lithium isopropoxide; sodium t-butanolate In 1,4-dioxane at 100℃; for 2h; Reagent/catalyst; Inert atmosphere; Schlenk technique;91%
With bis(tri-ortho-tolylphosphine)palladium(0); (R)-(-)-1-[(S)-2-(dicyclohexylphosphino)ferrocenyl]ethyl-di-tert-butylphosphine; ammonia; sodium t-butanolate In 1,4-dioxane at 100℃; for 24h; Inert atmosphere;89%
3095-47-4

3,5-dimethyl-4-aminobenzoic acid ethyl ester

87-62-7

2,6-dimethylaniline

Conditions
ConditionsYield
With potassium hydroxide In water at 60 - 125℃; under 2280.15 Torr; for 3h;97.5%
91-16-7

1,2-dimethoxybenzene

18109-39-2

N-(2,6-diimethylphenyl)benzamide

A

4038-14-6

3,4-dimethoxybenzophenone

B

87-62-7

2,6-dimethylaniline

Conditions
ConditionsYield
Stage #1: N-(2,6-diimethylphenyl)benzamide With 2-fluoropyridine; trifluoromethylsulfonic anhydride In dichloromethane at -78 - 0℃; for 0.166667h; Inert atmosphere;
Stage #2: 1,2-dimethoxybenzene In dichloromethane at 0 - 20℃; Inert atmosphere;
Stage #3: With hydrogenchloride; water In ethanol for 2h; Inert atmosphere; Reflux; chemoselective reaction;		A 97%
B 90%
576-26-1

2.6-dimethylphenol

87-62-7

2,6-dimethylaniline

Conditions
ConditionsYield
With 2,6-dimethylcyclohexanone; ammonium hydroxide; 5%-palladium/activated carbon at 180℃; for 5h; Concentration; Temperature;95.62%
With ammonia; hydrogen In 1,4-dioxane at 230℃; under 760.051 Torr;86.56%
With ammonia
39604-15-4

2,6-dimethylphenyl diethyl phosphate

87-62-7

2,6-dimethylaniline

Conditions
ConditionsYield
With potassium; potassium amide In diethyl ether; ammonia at -78℃; 1.0-1.2 h;95%

2,6-Dimethylaniline Chemical Properties

IUPAC Name: 2,6-dimethylaniline
Synonyms: 2,6-dimethyl-anilin;2,6-Dimethylbenzenamine;2,6-dimethylphenylamine;2,6-dimethyl-benzenamin;2,6-dimethyl-Benzenamine;2,6-Dimethylbenzeneamine;2,6-Dimethyl-phenylamine;2,6-DMA;
The Molecular formula of 2,6-Dimethylaniline(87-62-7): C8H11N
The Molecular Weight of 2,6-Dimethylaniline(87-62-7): 121.18
Molecular Structure : 
EINECS: 201-758-7
Melting point: 10-12 °C(lit.)
Boiling point: 216 °C
Flash point: 196 °F
density: 0.984 g/mL at 25 °C(lit.)
vapor pressure: <0.01 mm Hg ( 20 °C)
refractive index: n20/D 1.560(lit.)
Water Solubility: 7.5 g/L (20 oC)

2,6-Dimethylaniline Uses

2,6-Dimethylaniline(87-62-7) is used as a pesticide, pharmaceutical intermediate.

2,6-Dimethylaniline Toxicity Data With Reference

1、RTECS#: CAS# 87-62-7: ZE9275000 
2、LD50/LC50: RTECS: CAS# 87-62-7: Oral, mouse: LD50 = 707 mg/kg;Oral, rat: LD50 = 840 mg/kg;.
3、Carcinogenicity: 2,6-Dimethylaniline - California: carcinogen, initial date 1/1/91 IARC: Group 2B carcinogen
4、Other: See actual entry in RTECS for complete information.

2,6-Dimethylaniline Safety Profile

The Hazard Codes of 2,6-Dimethylaniline(87-62-7):  Xn,  N,  T
HazardClass: 6.1
The Risk Statements information of 2,6-Dimethylaniline(87-62-7):
40:  Limited evidence of a carcinogenic effect 
20/21/22:  Harmful by inhalation, in contact with skin and if swallowed 
37/38:  Irritating to respiratory system and skin 
51/53:  Toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment 
The Safety Statements information of 2,6-Dimethylaniline(87-62-7):
23:  Do not breathe gas/fumes/vapor/spray (appropriate wording to be specified by the manufacturer) 
25:  Avoid contact with eyes 
61:  Avoid release to the environment. Refer to special instructions safety data sheet 
36/37:  Wear suitable protective clothing and gloves 
RIDADR: UN 1711 6.1/PG 2
WGK Germany: 2
RTECS: ZE9275000
F: 8

2,6-Dimethylaniline Specification

(1):Fire Fighting Measures of 2,6-Dimethylaniline 
General Information: As in any fire, wear a self-contained breathing apparatus in pressure-demand, MSHA/NIOSH (approved or equivalent), and full protective gear. Will burn if involved in a fire. Containers may explode in the heat of a fire. Combustible liquid. 
Extinguishing Media: Use water spray to cool fire-exposed containers. Use water spray, dry chemical, carbon dioxide, or chemical foam.
(2):Accidental Release Measures of 2,6-Dimethylaniline
General Information: Use proper personal protective equipment as indicated in Section 8. 
Spills/Leaks: Absorb spill with inert material (e.g. vermiculite, sand or earth), then place in suitable container. Do not let this chemical enter the environment

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