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2-Amino-2'-fluoro-5-nitrobenzophenone

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Name

2-Amino-2'-fluoro-5-nitrobenzophenone

EINECS 206-454-8
CAS No. 344-80-9 Density 1.399 g/cm3
PSA 88.91000 LogP 3.65150
Solubility N/A Melting Point 158-160°C
Formula C13H9FN2O3 Boiling Point 485.6 °C at 760 mmHg
Molecular Weight 260.224 Flash Point 247.5 °C
Transport Information N/A Appearance yellow crystalline powder
Safety 24/25 Risk Codes N/A
Molecular Structure Molecular Structure of 344-80-9 (2-Amino-2'-fluoro-5-nitrobenzophenone) Hazard Symbols N/A
Synonyms

2-amino-5-nitro-2'-fluoro benzophenone;Benzophenone,2-amino-2'-fluoro-5-nitro- (7CI,8CI);2-Amino-5-nitro-2'-fluorobenzophenone;

 

2-Amino-2'-fluoro-5-nitrobenzophenone Synthetic route

2558-30-7

5-(2-fluorophenyl)-1,3-dihydro-7-nitro-2H-1,4-benzodiazepin-2-one

344-80-9

2-amino-5-nitro-2'-fluorobenzophenone

Conditions
ConditionsYield
With hydrogenchloride In ethanol Heating;
344-80-9

2-amino-5-nitro-2'-fluorobenzophenone

79-04-9

chloroacetyl chloride

2‑(2‑chloroacetamido)‑5‑nitro‑2′‑fluorobenzophenone

Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; for 12h;95%
623-73-4

diazoacetic acid ethyl ester

344-80-9

2-amino-5-nitro-2'-fluorobenzophenone

C17H15FN2O5

Conditions
ConditionsYield
With 1-methylimidazolium tetrafluoroborate In neat (no solvent) at 20℃; for 2h;90%
344-80-9

2-amino-5-nitro-2'-fluorobenzophenone

1138-80-3

N-(Benzyloxycarbonyl)glycine

Benzyl{[[2-(o-fluorobenzoyl)-4-nitrophenyl]carbamoyl]methyl}-carbamate

Conditions
ConditionsYield
With thionyl chloride; sodium hydrogencarbonate In tetrahydrofuran; ethyl acetate
1142-20-7

N-Cbz-Ala

344-80-9

2-amino-5-nitro-2'-fluorobenzophenone

59937-53-0

(S)-benzyl-{1-[[2-(o-fluorobenzoyl)-4-nitrophenyl]carbamoyl]ethyl}carbamate

Conditions
ConditionsYield
With thionyl chloride; sodium hydrogencarbonate In tetrahydrofuran
97-97-2

chloroacetaldehyde dimethyl acetal

344-80-9

2-amino-5-nitro-2'-fluorobenzophenone

59468-08-5

2-chloromethyl-4-(2-fluoro-phenyl)-6-nitro-1,2-dihydro-quinazoline 3-oxide

Conditions
ConditionsYield
With hydrogenchloride In ethanol
1142-20-7

N-Cbz-Ala

344-80-9

2-amino-5-nitro-2'-fluorobenzophenone

74892-38-9

(-)-benzyl-[1-[{2-(o-fluorobenzoyl)-4-nitrophenyl}-carbamoyl]ethyl]carbamate

Conditions
ConditionsYield
With phosphorus pentachloride In dichloromethane; toluene

2-(α-bromo-α-fluoroacetamido)-5-nitro-2'-fluorobenzophenone

359-22-8

bromo-fluoro-acetyl bromide

344-80-9

2-amino-5-nitro-2'-fluorobenzophenone

A

2-(α-amino-α-fluoroacetamido)-5-nitro-2'-fluorobenzophenone

B

60628-63-9

3-fluoro-5-o-fluorophenyl-7-nitro-2,3-dihydro-1H-1,4-benzodiazepin-2-one

Conditions
ConditionsYield
With hexamethylenetetramine In ethanol
344-80-9

2-amino-5-nitro-2'-fluorobenzophenone

7-amino-2-aminomethyl-1,3-dihydro-5-(2-fluorophenyl)-2H-1,4-benzodiazepine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: hydrogenchloride / ethanol
2: manganese dioxide / tetrahydrofuran; dichloromethane
3: acetic acid / nitromethane; dichloromethane; dimethyl sulfoxide
4: ethanol
View Scheme
344-80-9

2-amino-5-nitro-2'-fluorobenzophenone

1,3-dihydro-5-(2-fluorophenyl)-7-nitro-2-nitromethylene-2H-1,4-benzodiazepine 4-oxide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrogenchloride / ethanol
2: manganese dioxide / tetrahydrofuran; dichloromethane
3: acetic acid / nitromethane; dichloromethane; dimethyl sulfoxide
View Scheme

2-Amino-2'-fluoro-5-nitrobenzophenone Chemical Properties

Molecular Structure of Methanone,(2-amino-5-nitrophenyl)(2-fluorophenyl)- (CAS NO.344-80-9):

Molecular Formula: C13H9FN2O3
Molecular Weight: 260.2206
IUPAC Name: (2-Amino-5-nitrophenyl)-(2-fluorophenyl)methanone
Synonyms of Methanone,(2-amino-5-nitrophenyl)(2-fluorophenyl)- (CAS NO.344-80-9): EINECS 206-454-8 ; 2-Amino-2'-fluoro-5-nitrobenzophenone
CAS NO: 344-80-9
Classification Code: Aromatic Benzophenones & Derivatives (substituted) 
Index of Refraction: 1.638
Molar Refractivity: 66.82 cm3
Molar Volume: 185.8 cm3
Surface Tension: 59 dyne/cm
Density: 1.399 g/cm3
Flash Point: 247.5 °C
Enthalpy of Vaporization: 75.11 kJ/mol
Boiling Point: 485.6 °C at 760 mmHg
Vapour Pressure of Methanone,(2-amino-5-nitrophenyl)(2-fluorophenyl)- (CAS NO.344-80-9): 1.39E-09 mmHg at 25°C

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