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3-Methoxybenzyl alcohol

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Name

3-Methoxybenzyl alcohol

EINECS 230-200-5
CAS No. 6971-51-3 Density 1.085 g/cm3
PSA 29.46000 LogP 1.18750
Solubility Immiscible with water Melting Point 29 - 30oC
Formula C8H10O2 Boiling Point 247.4 °C at 760 mmHg
Molecular Weight 138.166 Flash Point 109.9 °C
Transport Information N/A Appearance Colorless to light yellow liquid
Safety 23-24/25-37/39-26-36 Risk Codes 36/37/38-22
Molecular Structure Molecular Structure of 6971-51-3 (m-Anisyl alcohol) Hazard Symbols HarmfulXn, IrritantXi
Synonyms

3-methoxy benzylalcohol;Benzylalcohol, m-methoxy- (6CI,7CI,8CI);(3-Methoxyphenyl)methanol;1-(Hydroxymethyl)-3-methoxybenzene;3-Methoxybenzenemethanol;NSC 66559;[3-(Methyloxy)phenyl]methanol;m-Anisalcohol;m-Methoxybenzyl alcohol;Benzenemethanol,3-methoxy-;

Article Data 187

3-Methoxybenzyl alcohol Synthetic route

591-31-1

3-methoxy-benzaldehyde

6971-51-3

3-methoxybenzyl alcohol

Conditions
ConditionsYield
With hydrogen; Pd as electrode electrochemical reaction;100%
With sodium tetrahydroborate In methanol at 20℃; for 1h;100%
With sodium tetrahydroborate; Dowex1-x8 In tetrahydrofuran at 20℃; for 0.5h;99%
5368-81-0

methyl 3-methoxybenzoate

6971-51-3

3-methoxybenzyl alcohol

Conditions
ConditionsYield
Stage #1: methyl 3-methoxybenzoate With diethylzinc; lithium chloride In tetrahydrofuran; hexane at 20℃; for 6h; Inert atmosphere;
Stage #2: With sodium hydroxide In tetrahydrofuran; hexane; water at 20℃; for 8h; Inert atmosphere; chemoselective reaction;
98%
With HN(CH2CH2C3H3N2Mes)2Cl2; potassium tert-butylate; hydrogen; cobalt(II) chloride In tetrahydrofuran at 100℃; under 22502.3 Torr; for 16h; Autoclave; Glovebox;91%
With methanol; sodium tetrahydroborate In tetrahydrofuran at 65℃; for 4h;90%
132816-03-6

(3-Methoxy-benzyloxy)-trimethyl-silane

6971-51-3

3-methoxybenzyl alcohol

Conditions
ConditionsYield
With Oxone In methanol for 0.4h; Heating;98%
With bismuth(lll) trifluoromethanesulfonate In methanol at 20℃; for 0.0333333h;97%
With poly (ethylene glycol)-sulfonated sodium montmorillonite nanocomposite In methanol at 20℃; for 0.00833333h;96%
18483-97-1

2-(3-methoxybenzyloxy)tetrahydro-2H-pyran

6971-51-3

3-methoxybenzyl alcohol

Conditions
ConditionsYield
With bismuth(lll) trifluoromethanesulfonate In methanol for 0.05h;97%
With sulfuric acid; silica gel In methanol at 20℃; for 0.5h;95%
With Oxone In methanol for 1.5h; Heating;80%
10259-22-0

ethyl 3-methoxybenzoate

6971-51-3

3-methoxybenzyl alcohol

Conditions
ConditionsYield
With lithium borohydride In diethyl ether; toluene at 100℃; for 0.5h;95%
1026136-92-4

2-tert-butylsulfinyl-3-methoxyphenylmethanol

6971-51-3

3-methoxybenzyl alcohol

Conditions
ConditionsYield
With nickel In ethanol for 3h; Reflux;94%
19693-78-8

2-(3-methoxyphenyl)-1,3-dioxolane

6971-51-3

3-methoxybenzyl alcohol

Conditions
ConditionsYield
With sulfuric acid; zinc at 38℃; for 2h; Temperature;93.5%
1058648-97-7

3-methoxy-1-[(ethoxymethoxy)methyl]benzene

6971-51-3

3-methoxybenzyl alcohol

Conditions
ConditionsYield
phosphotungstic acid In ethanol for 3h; Heating;93%
With 1-methylimidazole hydrogen sulfate at 50℃; for 1.25h; chemoselective reaction;92%
161358-52-7

3-methoxy-1-(methoxymethoxy)methyl benzene

6971-51-3

3-methoxybenzyl alcohol

Conditions
ConditionsYield
With 1-methylimidazole hydrogen sulfate at 120℃; for 0.05h; Microwave irradiation; chemoselective reaction;93%
phosphotungstic acid In ethanol for 3h; Heating;89%
591-31-1

3-methoxy-benzaldehyde

766-97-2

4-n-methylphenylacetylene

A

6971-51-3

3-methoxybenzyl alcohol

B

1-(3-methoxyphenyl)-3-(p-tolyl)prop-2-yn-1-one

Conditions
ConditionsYield
With triethylamine; zinc(II) iodide In toluene at 80℃; for 12h; Schlenk technique; Inert atmosphere;A n/a
B 93%

3-Methoxybenzyl alcohol Specification

1. Introduction of 3-Methoxybenzyl alcohol
3-Methoxybenzyl alcohol is clear colorless liquid for API intermediartes, the IUPAC Name of it is (3-Methoxyphenyl)methanol.

2. Properties of 3-Methoxybenzyl alcohol
Melting Point: 89-91 °C
Product Categories: Benzhydrols, Benzyl & Special Alcohols ; Alcohol 
Polar Surface Area: 18.46 Å2
Index of Refraction: 1.531
Molar Refractivity: 39.38 cm3
Molar Volume: 127.2 cm3
Surface Tension: 38.7 dyne/cm
Density of Benzenemethanol,3-methoxy-: 1.085 g/cm3
Flash Point: 109.9 °C
Enthalpy of Vaporization: 51.2 kJ/mol
Boiling Point: 247.4 °C at 760 mmHg
Vapour Pressure: 0.0136 mmHg at 25°C

3. Structure Descriptors of 3-Methoxybenzyl alcohol
InChI=1S/C8H10O2/c1-10-8-4-2-3-7(5-8)6-9/h2-5,9H,6H2,1H3 
InChIKey: IIGNZLVHOZEOPV-UHFFFAOYSA-N

4. Safety Information of 3-Methoxybenzyl alcohol

Hazard Codes : HarmfulXn,Xi
Risk Statements: 36/37/38-22 
R36/37/38: Irritating to eyes, respiratory system and skin. 
R22:Harmful if swallowed.
Safety Statements: 23-24/25-37/39-26-36 
S23: Do not breathe vapour. 
S24/25: Avoid contact with skin and eyes. 
S37/39: Wear suitable gloves and eye/face protection. 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36: Wear suitable protective clothing.
WGK Germany: 3
HS Code: 29094990

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