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Cas Database

Name	3-Hydroxybenzaldehyde	EINECS	202-892-9
CAS No.	100-83-4	Density	1.226 g/cm ³
PSA	37.30000	LogP	1.20470
Solubility	soluble in water	Melting Point	100-103 °C(lit.)
Formula	C₇H₆O₂	Boiling Point	240.9 °C at 760 mmHg
Molecular Weight	122.123	Flash Point	98.6 °C
Transport Information	N/A	Appearance	off-white solid
Safety	26-36-24/25	Risk Codes	36/37/38
Molecular Structure		Hazard Symbols	Xi
Synonyms	meta-Hydroxybenzaldehyde;Benzaldehyde, 3-hydroxy-;m-Formylphenol;3-Formylphenol;3-hydroxyBenzaldehyde;m-hydroxyBenzaldehyde;m-hydroxybenzaldehyde;Benzaldehyde, m-hydroxy-;	Article Data	172

3-Hydroxybenzaldehyde Synthetic route

: 620-24-6
3-Hydroxybenzyl alcohol

: 100-83-4
meta-hydroxybenzaldehyde

Conditions

Conditions	Yield
With silica gel; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium perchlorate In dichloromethane	100%
With manganese(IV) oxide; manganese(II) nitrate tetrahydrate; dibenzoyl peroxide In hexane at 70℃; under 760.051 Torr; for 0.0833333h; chemoselective reaction;	99%
In neat (no solvent) at 20℃; for 0.0333333h; Microwave irradiation;	99%

: Sodium; 6-{[1-(3-hydroxy-phenyl)-meth-(E)-ylidene]-amino}-hexanoate

: 100-83-4
meta-hydroxybenzaldehyde

Conditions

Conditions	Yield
With hydrogenchloride for 0.0416667h; Product distribution; Ambient temperature; pH = 4-6, regeneration of aldehyde;	100%

: 1700-37-4
3-Benzyloxybenzaldehyde

: 100-83-4
meta-hydroxybenzaldehyde

Conditions

Conditions	Yield
With iron(III) chloride on silica In neat (no solvent) at 80℃; for 0.5h;	99%
With magnesium iodide for 5h; neat (no solvent);	93%

: 96013-95-5
3-(tert-butyl-dimethyl-sylanyloxy)benzaldehyde

: 100-83-4
meta-hydroxybenzaldehyde

Conditions

Conditions	Yield
With lithium acetate In water; N,N-dimethyl-formamide at 25℃; for 8h; Inert atmosphere;	96%
With triethylamine N-oxide In methanol for 1h;	91%
In water; dimethyl sulfoxide at 90℃; for 8h;	87%

: 27004-28-0
2-(3-hydroxyphenyl)-1,3-dithiolane

: 100-83-4
meta-hydroxybenzaldehyde

Conditions

Conditions	Yield
With ammonium iodide; dihydrogen peroxide; sodium dodecyl-sulfate In water at 20℃; for 1h; micellar medium;	96%
With 2,4,4,6-Tetrabromo-2,5-cyclohexadien-1-one; dihydrogen peroxide In water; acetonitrile at 20℃; for 1h;	94%
With dihydrogen peroxide; iodine; sodium dodecyl-sulfate In water at 20℃; for 3h; Micellar solution;	90%

: 24393-20-2
2-(3-hydroxyphenyl)-1,3-dithiane

: 100-83-4
meta-hydroxybenzaldehyde

Conditions

Conditions	Yield
With dihydrogen peroxide; iodine; sodium dodecyl-sulfate In water at 20℃; for 0.666667h; Micellar solution;	95%
With acetic acid at 25℃; for 15h;	51%

: 13493-49-7
3-benzenesulfonyloxy-benzaldehyde

: 100-83-4
meta-hydroxybenzaldehyde

Conditions

Conditions	Yield
With potassium hydroxide In toluene; tert-butyl alcohol at 100℃; for 0.5h; Inert atmosphere;	95%

: 87199-16-4
3-Formylphenylboronic acid

: 100-83-4
meta-hydroxybenzaldehyde

Conditions

Conditions	Yield
With C100H52N4O16Sn(6-)*2In(3+); N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 3.5h; Irradiation;	94%
With C18H28Cl2CuN2O4 In water at 26℃; for 0.333333h;	92%
With 10-methylacridine-3(10H)-one; oxygen; N-ethyl-N,N-diisopropylamine In water at 20℃; for 20h; Irradiation; Green chemistry;	90%

: 40359-32-8
3-allyloxy-benzaldehyde

: 100-83-4
meta-hydroxybenzaldehyde

Conditions

Conditions	Yield
With bis(benzonitrile)palladium(II) dichloride In benzene for 20h; Heating;	92%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In methanol at 20℃; for 6h;	82%

: 817166-73-7
3-((triisopropylsilyl)oxy)benzaldehyde

: 100-83-4
meta-hydroxybenzaldehyde

Conditions

Conditions	Yield
With potassium acetate In water; N,N-dimethyl-formamide at 25℃; for 13h;	92%

3-Hydroxybenzaldehyde Chemical Properties

Product Name: 3-Hydroxybenzaldehyde
Synonyms: hydroxybenzaldehyde;m-Aldehydophenol;m-Formylphenol;m-hydroxy-benzaldehyd;3-hydroxy-benzaldehyd;Benzaldehyde, m-hydroxy-;HYDROXYBENZALDEHYDE-3; META-HYDROXY BENZALDEHYDE;
The Molecular formula of m-FORMYLPHENOL(100-83-4): C₇H₆O₂
The Molecular Weight of m-FORMYLPHENOL(100-83-4): 122.12
Molecular Structure :

EINECS: 202-892-9
Melting point: 100-103 °C(lit.)
Boiling point: 191 °C50 mm Hg(lit.)
Flash point: 191°C/50mm
Water Solubility: SOLUBLE
Sensitive: Air Sensitive
Appearance: Off-White Solid

3-Hydroxybenzaldehyde Toxicity Data With Reference

sce-hmn:lyms 1 mmol/L

MUREAV Mutation Research. 206 (1988),17.

3-Hydroxybenzaldehyde Consensus Reports

Reported in EPA TSCA Inventory.

3-Hydroxybenzaldehyde Safety Profile

Human mutation data reported. When heated to decomposition it emits acrid smoke and irritating vapors.
The Hazard Codes of m-FORMYLPHENOL(100-83-4):

Xi
The Risk Statements information of m-FORMYLPHENOL(100-83-4):
36/37/38: Irritating to eyes, respiratory system and skin
The Safety Statements information of m-FORMYLPHENOL(100-83-4):
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
24/25: Avoid contact with skin and eyes
WGK Germany: 3
RTECS: CU6450000
F: 8-9-23

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