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Cas Database |
| Name |
4-Chloro-3-nitrophenyl methyl sulfone |
EINECS | 202-557-7 |
| CAS No. | 97-07-4 | Density | 1.52 g/cm3 |
| PSA | 88.34000 | LogP | 3.25570 |
| Solubility | N/A | Melting Point |
125-129 ºC |
| Formula | C7H6ClNO4S | Boiling Point | 414.179 °C at 760 mmHg |
| Molecular Weight | 235.648 | Flash Point | 204.288 °C |
| Transport Information | N/A | Appearance | N/A |
| Safety | Risk Codes | R20/21/22; R36/37/38 | |
| Molecular Structure |
|
Hazard Symbols |
 Xn
|
| Synonyms |
Sulfone,4-chloro-3-nitrophenyl methyl (6CI,7CI,8CI);1-Chloro-4-(methylsulfonyl)-2-nitrobenzene;2-Chloro-5-(methylsulfonyl)-1-nitrobenzene;3-Nitro-4-chlorophenyl methyl sulfone;4-(Methylsulfonyl)-2-nitrochlorobenzene;NSC 25818; |
Article Data | 7 |
4-Chloro-3-nitrophenyl methyl sulfone Synthetic route
| Conditions | Yield |
|---|---|
| With sulfuric acid; nitric acid at 25℃; for 2h; | 99.7% |
| (nitration); |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1.1: sodium sulfite; sodium hydrogencarbonate / water / 4 h / 75 °C 1.2: 15 h / 105 - 107 °C 2.1: sulfuric acid; nitric acid / 2 h / 25 °C View Scheme |
- 97-07-4
1-chloro-4-methanesulfonyl-2-nitrobenzene
- 917562-22-2
C12H13NO8S
| Conditions | Yield |
|---|---|
| Stage #1: malonic acid dimethyl ester With potassium tert-butylate In tert-butyl alcohol Stage #2: 1-chloro-4-methanesulfonyl-2-nitrobenzene In tert-butyl alcohol at 20℃; for 15h; Heating / reflux; | 100% |
| Conditions | Yield |
|---|---|
| In ethanol at 40 - 80℃; for 0.5h; | 99% |
| With sodium hydroxide |
| Conditions | Yield |
|---|---|
| With sodium hydroxide In dimethyl sulfoxide at 60℃; for 1h; | 96% |
- 97-07-4
1-chloro-4-methanesulfonyl-2-nitrobenzene
- 616-30-8, 13552-31-3
3-Amino-1,2-propanediol
- 120381-40-0
4-(β,γ-dihydroxypropylamino-3-nitro)phenyl methyl sulfone
| Conditions | Yield |
|---|---|
| In dimethyl sulfoxide | 95% |
- 97-07-4
1-chloro-4-methanesulfonyl-2-nitrobenzene
- 2557-78-0
2-fluorothiophenol
- 129846-91-9
2-(2-fluorophenylthio)-5-(methylsulfonyl)nitrobenzene
| Conditions | Yield |
|---|---|
| With potassium carbonate In acetone at 20℃; for 4h; | 95% |
- 97-07-4
1-chloro-4-methanesulfonyl-2-nitrobenzene
- 693-05-0
N-(2-cyanoethyl)-N-methylamine
- 81689-46-5
3-[(4-Methanesulfonyl-2-nitro-phenyl)-methyl-amino]-propionitrile
| Conditions | Yield |
|---|---|
| In butan-1-ol at 118℃; for 2h; | 91% |
| Conditions | Yield |
|---|---|
| With tert.-butylhydroperoxide; hydrogen In water; toluene at 160℃; under 30003 Torr; for 36h; Autoclave; | 84% |
- 97-07-4
1-chloro-4-methanesulfonyl-2-nitrobenzene
- 39930-15-9
(3-chlorophenyl)(pyridin-2-yl)methanamine
| Conditions | Yield |
|---|---|
| With N-ethyl-N,N-diisopropylamine In N,N-dimethyl acetamide at 130℃; for 0.5h; Sealed tube; Microwave irradiation; | 83% |
4-Chloro-3-nitrophenyl methyl sulfone Chemical Properties
Molecular Structure:
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Molecular Formula: C7H6ClNO4S
Molecular Weight: 235.6448
IUPAC Name: 1-Chloro-4-methylsulfonyl-2-nitrobenzene
Synonyms of 4-Chloro-3-nitrophenyl methyl sulfone (CAS NO.97-07-4): 3-Nitro-4-chlorophenyl methyl sulfone ; EINECS 202-557-7 ; NSC 25818 ; 1-Chloro-4-(methylsulphonyl)-2-nitrobenzene ; Benzene, 1-chloro-4-(methylsulfonyl)-2-nitro- ; Sulfone, 4-chloro-3-nitrophenyl methyl (8CI)
CAS NO: 97-07-4
Product Categories: Benzene derivates
Index of Refraction: 1.572
Molar Refractivity: 51.05 cm3
Molar Volume: 155 cm3
Surface Tension: 52.6 dyne/cm
Density: 1.52 g/cm3
Flash Point: 204.3 °C
Enthalpy of Vaporization: 64.12 kJ/mol
Boiling Point: 414.2 °C at 760 mmHg
Vapour Pressure of 4-Chloro-3-nitrophenyl methyl sulfone (CAS NO.97-07-4): 1.09E-06 mmHg at 25°C
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