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Cas Database |
| Name |
8-NITROQUINOLINE |
EINECS | 210-135-9 |
| CAS No. | 607-35-2 | Density | 1.354 g/cm3 |
| PSA | 58.71000 | LogP | 2.66620 |
| Solubility | Soluble in ethanol, ethyl ether and benzene, slightly soluble in cold water. | Melting Point |
89-91 °C(lit.) |
| Formula | C9H6N2O2 | Boiling Point | 323.1 °C at 760 mmHg |
| Molecular Weight | 174.159 | Flash Point | 149.2 °C |
| Transport Information | N/A | Appearance | white to light yellow crystal powder |
| Safety | 26-27-36/37/39-36 | Risk Codes | 20/21/22-36/37/38-40-68 |
| Molecular Structure |
|
Hazard Symbols |
 Xn,  Xi
|
| Synonyms |
8-Nitroqunioline;quinoline, 8-nitro-;5-20-07-00327 (Beilstein Handbook Reference); |
Article Data | 37 |
8-NITROQUINOLINE Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide; [bis(trifluoroacetoxy)iodo]benzene; sodium nitrite In acetonitrile at 20℃; for 3h; regioselective reaction; | 84% |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 2-nitro-aniline; glycerol With sodium iodide at 20℃; for 0.0833333h; Stage #2: With sulfuric acid for 0.166667h; Cooling with ice; Stage #3: at 140℃; for 2h; | 81% |
| Stage #1: 2-nitro-aniline With sulfuric acid at 70 - 80℃; Stage #2: glycerol at 70 - 80℃; Temperature; Further stages; | 79% |
| With sulfuric acid In water for 4h; Reflux; | 72% |
- 39217-93-1
8-nitro-1,2,3,4-tetrahydroquinoline
- 607-35-2
8-nitroquinoline
Conditions
| Conditions | Yield |
|---|---|
| With iodine; oxygen In 1,2-dichloro-benzene; toluene at 160℃; for 30h; | 77% |
Conditions
| Conditions | Yield |
|---|---|
| With sulfuric acid In water; glycerol Reflux; | 44% |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: quinoline With sulfuric acid; nitric acid at 20℃; for 1h; Stage #2: With sodium carbonate In water | A 34% B 38% |
| With sulfuric acid; nitric acid In water at 0 - 20℃; for 1h; | A 35% B n/a |
| With sulfuric acid; nitric acid |
Conditions
| Conditions | Yield |
|---|---|
| durch Nitrieren; |
- 607-35-2
8-nitroquinoline
Conditions
| Conditions | Yield |
|---|---|
| With ammonia at 130 - 140℃; im Rohr; |
Conditions
| Conditions | Yield |
|---|---|
| With phosphoric acid; water; orthoarsenic acid | |
| With hydrogenchloride; phosphoric acid In water at 80 - 95℃; for 7h; |
Conditions
| Conditions | Yield |
|---|---|
| With nitric acid at 160℃; im Rohr; |
8-NITROQUINOLINE Chemical Properties
The molecular formula of 8-Nitroquinoline(607-35-2) is C9H6N2O2 and its formula weight is 174.16.
8-Nitroquinoline(607-35-2) has a melting point of 89-91 °C(lit.).
The chemical synonyms of 8-Nitroquinoline(607-35-2) are 8-nitro-quinolin;Quinoline, 8-nitro-;Quinoline,8-nitro-;AKOS 214-03;8-NITROQUINOLINE;8-Nitroqunioline;8-Nitroquinoline,98%;8-Nitrochinolin
The molecular structure of 8-Nitroquinoline(607-35-2):
8-Nitroquinoline(607-35-2) has a melting point of 89-91 °C(lit.).
The chemical synonyms of 8-Nitroquinoline(607-35-2) are 8-nitro-quinolin;Quinoline, 8-nitro-;Quinoline,8-nitro-;AKOS 214-03;8-NITROQUINOLINE;8-Nitroqunioline;8-Nitroquinoline,98%;8-Nitrochinolin
The molecular structure of 8-Nitroquinoline(607-35-2):
8-NITROQUINOLINE Toxicity Data With Reference
| 1. | mmo-sat 50 µg/plate | MUREAV Mutation Research. 39 (1977),285. | ||
| 2. | mma-sat 100 nmol/plate | MUREAV Mutation Research. 58 (1978),11. | ||
| 3. | dnr-sat 350 µg/disc | MUREAV Mutation Research. 39 (1977),285. | ||
| 4. | orl-rat TD:36,400 mg/kg/2Y-C:CAR,REP | CALEDQ Cancer Letters (Shannon, Ireland). 14 (1981),115. | ||
| 5. | ipr-mus LDLo:125 mg/kg | CBCCT* “Summary Tables of Biological Tests“ National Research Council Chemical-Biological Coordination Center. 6 (1954),149. |
8-NITROQUINOLINE Consensus Reports
EPA Genetic Toxicology Program. Reported in EPA TSCA Inventory.
8-NITROQUINOLINE Safety Profile
Poison by intraperitoneal route. Experimental reproductive effects. Questionable carcinogen with experimental carcinogenic data. Mutation data reported. When heated to decomposition it emits toxic fumes of NOx. See also 2-NITROQUINOLINE; 5-NITROQUINOLINE; 6-NITROQUINOLINE; 4-NITROQUINOLINE-N-OXIDE.
Hazard Codes Xn,Xi
Risk Statements 20/21/22-36/37/38-40-68
Safety Statements 26-27-36/37/39-36
WGK Germany 3
RTECS VC1925000
Hazard Note Harmful/Irritant
Hazard Codes Xn,Xi
Risk Statements 20/21/22-36/37/38-40-68
Safety Statements 26-27-36/37/39-36
WGK Germany 3
RTECS VC1925000
Hazard Note Harmful/Irritant
8-NITROQUINOLINE Specification
Chemical Stability: Not available
Conditions to Avoid: Incompatible materials.
Incompatibilities with Other Materials Strong oxidizing agents, strong acids, strong bases.
Hazardous Decomposition Products Nitrogen oxides, carbon monoxide, carbon dioxide.
Hazardous Polymerization Has not been reported.
Conditions to Avoid: Incompatible materials.
Incompatibilities with Other Materials Strong oxidizing agents, strong acids, strong bases.
Hazardous Decomposition Products Nitrogen oxides, carbon monoxide, carbon dioxide.
Hazardous Polymerization Has not been reported.
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8-Nitroquinoline
