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Cas Database

Name	Amylamine	EINECS	203-780-2
CAS No.	110-58-7	Density	0.755 g/cm³
PSA	26.02000	LogP	1.83560
Solubility	soluble	Melting Point	-55 °C(lit.)
Formula	C₅H₁₃N	Boiling Point	105.5 °C at 760 mmHg
Molecular Weight	87.1649	Flash Point	4.4 °C
Transport Information	UN 1106 3/PG 2	Appearance	clear colourless to very slightly yellow liquid
Safety	16-26-36/37/39-45-33	Risk Codes	11-22-34-42/43-20/21/22
Molecular Structure		Hazard Symbols	F,C
Synonyms	Pentylamine(8CI);1-Aminopentane;1-Pentylamine;Monoamylamine;Monopentylamine;NSC 7906;Norleucamine;n-Amylamine;n-Pentylamine;1-Pentanamine;	Article Data	130

Amylamine Synthetic route

: 110-59-8
pentanonitrile

: 110-58-7
1-pentanamine

Conditions

Conditions	Yield
With borane-ammonia complex; C15H30Cl2CoN3P In hexane at 120℃; for 16h; Sealed tube; Inert atmosphere; chemoselective reaction;	86%
With hydrogen; sodium methylate; nickel In methanol hydrogen generated in situ electrochemically on Raney nickel electrode;	72%
With lithium aluminium tetrahydride	71%

: 110-62-3
pentanal

: 110-58-7
1-pentanamine

Conditions

Conditions	Yield
With ammonia; hydrogen In methanol at 30℃; for 15h; Autoclave;	94%
With ammonium hydroxide; ammonium acetate; hydrogen; [Ru(cod)Cl]2; trisodium tris(3-sulfophenyl)phosphine In toluene at 145℃; under 48754.9 Torr; for 10h;	47 % Chromat.
With ammonium hydroxide; hydrogen at 65℃; under 11251.1 Torr; for 12h; Autoclave; Green chemistry;
With pyridoxal 5'-phosphate; Amine transaminase 117; rac-methylbenzylamine; N-2-hydroxyethylpiperazine-N'-2-ethanesulfonic acid In water; dimethyl sulfoxide at 30℃; Reagent/catalyst; Enzymatic reaction;

: 26330-06-3
pentyl azide

: 110-58-7
1-pentanamine

Conditions

Conditions	Yield
With hydrogen; MCM-silylamine Pd(II) In methanol at 20℃; for 2h; Reduction;	90%

: 1119-46-6
5-chloro-valeric acid

A: 110-89-4
piperidine

B: 675-20-7
piperidin-2-one

C: 110-58-7
1-pentanamine

D: 109-73-9
N-butylamine

Conditions

Conditions	Yield
Stage #1: 5-chloro-valeric acid With cyclopentyl methyl ether; ammonia at 200℃; under 4500.45 Torr; Sealed tube; Green chemistry; Stage #2: With cyclopentyl methyl ether; ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6.5h; Cooling with ice; Green chemistry;	A 85% B 9% C 2% D 2%

: 628-02-4
Caproamide

: 110-58-7
1-pentanamine

Conditions

Conditions	Yield
With sodium hydroxide; benzyltrimethylazanium tribroman-2-uide In water at 70℃; for 2h;	80%
With sodium hydroxide; sodium bromite In water at 75℃; for 0.5h;	60%
With sodium hypochlorite

: 71-41-0
pentan-1-ol

A: 110-58-7
1-pentanamine

B: 109-52-4
valeric acid

Conditions

Conditions	Yield
With carbonylchlorohydrido(4,5-bis((diisopropylphosphino)methyl)acridine)ruthenium(II); ammonia; water In 1,4-dioxane at 135℃; under 5700.38 Torr; for 30h; Inert atmosphere;	A 70.0 %Chromat. B n/a

: 60169-95-1
N,N'-dipentyl-oxalamide

: 110-58-7
1-pentanamine

Conditions

Conditions	Yield
With potassium tert-butylate; hydrogen; [Ru(PtBuNNHBn)H(CO)Cl] In toluene at 135℃; under 30003 Torr; for 24h;	97 %Spectr.

: 5775-76-8, 5780-42-7, 628-79-5
valeraldoxime

: 110-58-7
1-pentanamine

Conditions

Conditions	Yield
With ethanol; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation;
With diethyl ether; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation;
With palladium on activated charcoal; acetic acid Hydrogenation;

: 5775-76-8, 5780-42-7, 628-79-5
valeraldoxime

A: 110-58-7
1-pentanamine

B: 2050-92-2
Di-n-amylamine

Conditions

Conditions	Yield
With nickel kieselguhr; methyl cyclohexane at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation;
With diethyl ether; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation;
With ethanol; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation;

: 628-02-4
Caproamide

A: 110-58-7
1-pentanamine

B: 142-62-1
hexanoic acid

Conditions

Conditions	Yield
With sodium hydroxide; sodium persulfate; sodium chloride In water at 85 - 90℃; for 7h;	A 36% B 56%
With sodium hydroxide; sodium persulfate; copper dichloride In water at 85 - 90℃; for 7h;	A 36% B 56%
With sodium hydroxide; sodium persulfate; sodium chloride In water at 85 - 90℃; for 7h;	A 36% B 52%
With sodium hydroxide; sodium persulfate; sodium chloride In water at 85 - 90℃; for 7h;	A 36% B 52%

Amylamine Chemical Properties

Molecular Formula: C₅H₁₃N

Molecular Weight: 87.16
Density: 0.755
Melting point: -50 ^oC
Boiling point: 104 ^oC
VAPOR DENSITY: 3.0
AUTOIGNITION: 435 ^oC
FLASH POINT: 20 ^oC
Refractive index: 1.41-1.412
Flash point: 4 ^oC
Water solubility: soluble
Soluble: alcohol
PHYSICAL STATE OF Amylamine (110-58-7): clear liquid
ODOR OF Amylamine (110-58-7): ammonia odor

Amylamine Uses

Amylamine (110-58-7) can be used for medicine, dyes, emulsifiers, thiofide, anticorrosive agent, flotation agent and so on.

Amylamine Production

In the presence of catalyst, sodium azide reacts with caproic acid. After alkali neutralization, wet distillation and then extracting distillate by aether. Extract liquor is refined to Amylamine (110-58-7) by ectification.

Amylamine Toxicity Data With Reference

ipr-rat LDLo:37,500 µg/kg

FATOAO Farmakologiya i Toksikologiya (Moscow). 31 (1968),238.

Amylamine Consensus Reports

Reported in EPA TSCA Inventory.

Amylamine Safety Profile

Hazard Symbols: F;C (Flammable; Corrosive)
Risk Codes: R11;R20/21/22;R34 (Highly flammable; Harmful by inhalation, in contact with skin and if swallowed; Causes burns.)
Safety Description: S16;S26;S36/37/39;S45 (Keep away from sources of ignition; In case of contact with eyes, rinse immediately with plenty of water and seek medical advice; Wear suitable protective clothing, gloves and eye/face protection; In case of accident or if you feel unwell, seek medical advice immediately)
Transport Information: UN 1106
Poison by intraperitoneal route. A corrosive. A flammable liquid. When heated to decomposition it emits toxic vapors of NO_x.

Amylamine Standards and Recommendations

DOT Classification: 8; Label: Corrosive, Flammable Liquid (UN 2734); DOT Class: 3; Label: Flammable Liquid, Corrosive (UN 2733)
PURITY (GC): 98.0% min
SPECIFIC GRAVITY: 0.75 - 0.76
MOISTURE: 0.1% max
COLOR (AHHA): 30 max

Amylamine Specification

STORAGE: Store with flammable liquids. Store outside or in a detached building. Keep separated from incompatible substances. Protect from physical damage. Avoid heat, flames, sparks and other sources of ignition.

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