cas 115186-31-7, N-Boc-N'-Fmoc-D-lysine | Articles data ｜lookchem

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115186-31-7

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Solution phase synthesis of β-peptides using micro reactors
The synthesis of β-peptides has been successfully performed using a borosilicate glass micro reactor, in which a network of channels has been produced using a photolithographic and wet etching method. The reagents were mobilised by electroosmotic flow (EOF). The micro reactor was initially evaluated using a carbodiimide coupling reaction to form a dipeptide. The methodology has been extended such that the peptides may also be produced via the pentafluorophenyl ester derivatives of amino acids. It was found that performing the pentafluorophenyl ester reactions in the micro reactor resulted in an increase in the reaction efficiency over the traditional batch method. We postulate that the enhancement in rate of reaction is an electrochemical phenomenon, due to the reaction being performed in an electric field, which is unique to micro reactor systems. It has also been demonstrated that selective deprotection of the resultant dipeptides can be achieved. This approach has been used in the synthesis of a tripeptide.
Watts, Paul,Wiles, Charlotte,Haswell, Stephen J,Pombo-Villar, Esteban
p. 5427 - 5439
(2007/10/03)

Solid-Phase Total Synthesis of Oscillamide Y and Analogues
We report an efficient solid phase synthesis of oscillamide Y and three analogues. The cyclic peptide was prepared using a combination of Fmoc and allyl chemistries and an acid labile Wang type linker. The urea functionality was smoothly incorporated usin
Marsh, Ian R.,Bradley, Mark,Teague, Simon J.
p. 6199 - 6203
(2007/10/03)

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850863-77-3
Nα-(4-nitrophenyloxycarbonyl)-Nε-(9-fluorenylmethoxycarbonyl)-D-Lys allyl ester

Chemical Properties

Melting Point: 117-123℃
Boiling Point: 685.7oC at 760 mmHg
Flash Point:368.5oC
Density: 1.21g/cm3
Storage Temp.:Store at RT.
Vapor Pressure: 9.55E-20mmHg at 25°C
PKA: 3.99±0.21(Predicted)
PSA: 113.96000
LogP: 5.45510

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