Highly stereoselective synthesis of 2,3-unsaturated thioglycopyranosides employing molecular iodine
Molecular iodine has been utilized for the first time for the thioglycosidation of d-glycals with various thiols to afford the corresponding 2,3-unsaturated thioglycosides in high yields. In the case of tri-O-acetyl-d-glucal, the -anomer was obtained exclusively. The use of readily available iodine makes this method quite simple, more convenient, and practical. Georg Thieme Verlag Stuttgart.
Reddy, Basi V. Subba,Divyavani,Yadav, Jhillu S.
experimental part
p. 1617 - 1620
(2010/06/20)
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