Fluorinated ketene dithioacetals; 1. Preparation and application to the synthesis of α-trifluoromethylthiocarboxylic S-esters and aldehyde derivatives
α-Trifluoromethylketene dithioacetals 3 were synthesized by Peterson reaction from trifluoromethyl ketones 1 and trimethylsilyl dithioacetals 2. Acid hydrolysis and reduction yield α-trifluoromethylthiocarboxylic S-esters 4 and α-trifluoromethyl dithioace
Muzard,Portella
p. 965 - 968
(2007/10/02)
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