cas 15147-64-5, 2,3-Dinitrobenzoic acid | Articles data ｜lookchem

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15147-64-5

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A green, reusable and highly efficient solid acid catalyst for the oxidation of aldehydes to the corresponding carboxylic acids using H 2O2 and KMnO4:H5PV 2Mo10O40 (10-molybdo-2-vanadophosphoric heteropolyacid)
H5PV2Mo10O40-catalyzed oxidation of aromatic aldehydes to the corresponding carboxylic acids using hydrogen peroxide and KMnO4 as oxidants under mild conditions is reported. This system provides an efficient, convenient and practical method for the oxidation of aromatic aldehydes. In this work, differences between Keggin and Well-Dawson type polyoxometalates are addressed in term of relative stability, hardness and acidity.
Shojaei, Abdollah Fallah,Rezvani, Mohamad Ali,Heravi, Majid
experimental part
p. 1513 - 1522
(2012/03/08)

Electrophilic Aromatic Substitution. Part 37. Products of Aromatic Nitrations of some Chloronitrobenzenes and Substituted Benzoic Acids in Solutions of Dinitrogen Pentaoxide and of Nitronium Salts in Nitric Acid
Yields of aromatic products of nitration in nitric acid solutions containing dinitrogen pentaoxide or nitronium salt have been determined.Evidence for the intrusion of a mechanism other than the normal nitronium ion one comes from comparison of products in the two media and from the observation of 15N NMR CIDPN effects.The additional mechanism operative with some substrates in concentrated solutions of dinitrogen pentaoxide is postulated to be one in which reversible addition of the NO3 radical is followed by combination with NO2.Dienes produced in this way can give aromatic nitroproducts by elimination of nitric acid.Nitrodecarboxylation of substituted benzoic acids occurs by a radical process.
Moodie, Roy B.,Sanderson, Andrew J.,Willmer, Richard
p. 645 - 650
(2007/10/02)

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Chemical Properties

Boiling Point: 440.2 °C at 760 mmHg
Flash Point:199.9 °C
Density: 1.688 g/cm³
Vapor Pressure: 1.58E-08mmHg at 25°C
Refractive Index: 1.658
PKA: pK1:1.85 (25°C)
PSA: 128.94000
LogP: 2.24760

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