- One-pot electrochemical synthesis of acid anhydrides from alcohols
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One-pot indirect electrochemical oxidation of alcohols in the methylene chloride–aqueous solution of sodium hydrocarbonate two-phase system in the presence of potassium iodide, 4-acetylamino-2,2,6,6-tetramethylpiperidin-1-oxyl, and 2,6-lutidine results in
- Kashparova,Papina,Kashparov,Zhukova, I. Yu.,Ilchibaeva,Kagan, E. Sh.
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p. 2733 - 2735
(2017/12/26)
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- Synthesis of alkyl aryl ketones by Pd/light induced carbonylative cross-coupling of alkyl iodides and arylboronic acids
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Alkyl aryl ketones were synthesized by the carbonylative cross-coupling reaction of alkyl iodides and arylboronic acids under combined Pd/light conditions. In this reaction, it is likely that an acylpalladium species would be formed via carbonylation of t
- Sumino, Shuhei,Ui, Takahito,Ryu, Ilhyong
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p. 3142 - 3145
(2013/07/26)
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- Synthesis of alkyl alkynyl ketones by Pd/light-induced three-component coupling reactions of iodoalkanes, CO, and 1-alkynes
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Under photoirradiation conditions using xenon light, in the presence of a catalytic amount of PdCl2(PPh3)2 with triethylamine as a base, a three-component coupling reaction of iodoalkanes, carbon monoxide, and terminal alkynes proceeded to give alkyl alkynyl ketones in good yields.
- Fusano, Akira,Fukuyama, Takahide,Nishitani, Satoshi,Inouye, Takaya,Ryu, Ilhyong
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supporting information; experimental part
p. 2410 - 2413
(2010/07/17)
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- REACTION OF PHOSPHORUS TRICHLORIDE WITH CARBOXYLIC ACIDS
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The reaction of phosphorus trichloride with a number of monobasic carboxylic acids has been studied and the optimum ratio of reactants for the yield of acid chlorides has been established.Based on analysis and the data from 31P NMR spectroscopy of the phosphorus-containing products from this reaction it is shown that at 40-50 deg C a mixture of P-H acids having a predominant content of pyrophosphorous acid is formed.
- Valitova, L. A.,Popova, E. V.,Ibragimov, Sh. N.,Ivanov, B. E.
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p. 366 - 370
(2007/10/02)
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