Synthesis and axial chirality of an enantiopure aminodibenzazepinone
A route for the synthesis of (S,S)-7-amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-one hydrochloride is disclosed. The synthesis includes a Friedel-Crafts alkylation to form the seven-membered ring and a highly efficient classical resolution. Additional stud
Cole, Kevin P.,Mitchell, David,Austin Carr,Stout, James R.,Belvo, Matthew D.
experimental part
p. 1262 - 1266
(2009/12/01)
Polycyclic α-amino-ε-caprolactams and related compounds
Disclosed are polycyclic α-amino-ε-caprolactams and related compounds which are useful as synthetic intermediates in the preparation of inhibitors of β-amyloid peptide release and/or its synthesis.
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Page/Page column 36; 39
(2010/02/14)
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