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3073-87-8

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Development of a method for the synthesis of 2,4,5-trisubstituted oxazoles composed of carboxylic acid, amino acid, and boronic acid
A novel method for the synthesis of trisubstituted oxazoles via a one-pot oxazole synthesis/Suzuki–Miyaura coupling sequence has been developed. One-pot formation of 5-(triazinyloxy)oxazoles using carboxylic acids, amino acids and a dehydrative condensing reagent, DMT-MM, followed by Ni-catalyzed Suzuki–Miyaura coupling with boronic acids provided the corresponding 2,4,5-trisubstituted oxazoles in good yields.
Yamada, Kohei,Kamimura, Naoto,Kunishima, Munetaka
p. 1478 - 1485
(2017/08/02)

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Chemical Properties

Appearance/Colour :yellow needles with a blue fluorescence
Melting Point: 233-235 °C(lit.)
Boiling Point: 571.7°Cat760mmHg
Flash Point:290.6°C
Density: 1.17g/cm³
Vapor Pressure: 1.74E-12mmHg at 25°C
Refractive Index: 1.5300 (estimate)
PKA: 0.76±0.10(Predicted)
BRN: 629905
PSA: 52.06000
LogP: 6.94740

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