SYNTHESIS OF UNSYMMETRICAL 1,1-DIALKOXYALKANES AND THEIR SULFUR-CONTAINING ANALOGS
Acyclic acetals and 1,1-di(alkylthio)alkanes enter into exchange reactions in the presence of aprotic acids and of the KU-2 cation-exchange resin with the formation of the unsymmetric acetals and 1-alkoxy-1-alkylthioalkanes.In reaction with ethylal di(ethylthio)methane forms 3,5,7-trioxanonane in addition to ethylthioethoxymethane. 2-Methyl-4-thia-2-hexene was found in the products from the reaction of 1,1-di(ethylthio)-2-methylpropane with methylal.
Gazizova, L. B.,Imashev, U. B.,Musavirov, R. S.,Kantor, E. A.,Zlotskii, S. S.,et al.
p. 226 - 231
(2007/10/02)
SYNTHESIS AND REACTIONS OF 1,1-BIS(ETHYLTHIO)ALKANES
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Musavirov, R. S.,Gazizova, L. B.,Nedogrei, E. P.,Kantor, E. A.,Zlot-skii, S. S.,Rakhmankulov, D. L.
p. 889 - 892
(2007/10/02)
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