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4430-15-3

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A selective solvent-free self-condensation of carbonyl compounds utilizing microwave irradiation
An environmentally benign microwave-assisted solvent-free self-condensation of carbonyl compounds was developed using catalytic amounts of triethylamine and lithium perchlorate. Changing the amount of lithium perchlorate helps in controlling the ratio of the single-condensation and double-condensation products. The effect of other additives and microwave activation was also investigated. The optimized conditions were then applied to various cyclic/acyclic ketones and aldehydes, with selectivity observed in many cases.
Sharma, Lalit Kumar,Kim, Kyung Bo,Elliott, Gregory I.
supporting information; experimental part
p. 1546 - 1549
(2011/07/31)

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548-35-6
truxene

Chemical Properties

Melting Point: >300 °C(lit.)
Boiling Point: 706.6±50.0 °C(Predicted)
Density: 1.503±0.06 g/cm3(Predicted)
PSA: 51.21000
LogP: 4.99980

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