Simple one pot synthesis of ketone from carboxylic acid using DCC as an activator
Simple one pot procedure for the conversion of carboxylic acid to ketone is described. Various carboxylic acids were converted to the corresponding ketones in excellent manner in presence of N,N′-dicyclohexylcarbodiimide (DCC) and organometallic reagents. Aromatic, heteroaromatic and aliphatic acids were converted to the corresponding ketones smoothly under the optimum conditions using organolithium reagents. In this process, desired products have been isolated from the crude reaction mixtures in moderate yields during the purification process.
Mekonnen, Habtamu Gelaw,Jana, Samaresh
supporting information
p. 1382 - 1384
(2019/04/30)
1,3-Dithiane polymers for the supported synthesis of ketones
The synthesis of polymeric reagents containing an odorless propane-1,3- dithiol functionality is reported. Their usefulness for the solid phase synthesis of ketones via the umpoled alkylation of 1,3-dithianes is demonstrated.
Bertini, Vincenzo,Lucchesini, Francesco,Pocci, Marco,De Munno, Angela
p. 9263 - 9266
(2007/10/03)
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