cas 64394-45-2, 1,3,4,6-TETRATHIAPENTALENE-2,5-DIONE | Articles data ｜lookchem

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64394-45-2

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Noncoupling Synthesis of Tetrathiafulvalenes
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Schumaker, R. R.,Lee, V. Y.,Engler, E. M.
p. 564 - 566
(1984)
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[1,3]-Dithiolo-[4,5-d ][1,3-dithiole]-2,5-dione
A safe, three-step reaction sequence to [1,3]-dithiolo-[4,5- d ][1,3-dithiole]-2,5-dione starting from carbon disulfide is presented. Optimized reaction conditions, rigorous purification, and full characterization of all intermediates provide reproducibly a final product of superior quality with a melting point of 181 °C (dec.).
Müller, Harald,Bourcet, Léa
p. 1817 - 1822
(2021/11/04)

TRANSITION-METAL 1,2-DIHETEROLENES AND POLYHETEROTETRAHETERAFULVALENES: PRECURSORS OF CONDUCTING SOLIDS
Methods for synthesis and properties of oxygen-, sulfur-, selenium-, and nitrogen-containing transition-metal 1,2-diheterolenes and polyheterotetraheterafulvalenes are described.Also, the preparation and properties of some conducting salts based on these compounds are briefly discussed.
Papavassiliou, G. C.,Kakoussis, V. C.,Lagouvardos, D. J.,Mousdis, G. A.
p. 171 - 184
(2007/10/02)

Tetrathiafulvalenes. XIX. Synthesis and Properties of Electron Conducting Poly-Dithiolene Complexes with Ethylene Tetrathiolat and Tetrathiafulvalene Tetrathiolat as Bridge Ligands
-Dithiolo-1,3-dithiol-2,5-dione 7 and 5-(5-oxo-dithiolo-1,3-dithiole-2-ylidene)-dithiolo-1,3-dithiol-2-one 8 were synthesized from 1,3-dithiole-2-thione-4,5-dithiolat.The ligands react with salts of iron, cobalt, nickel
Poleschner, H.,John, W.,Hoppe, F.,Fanghaenel, E.
p. 957 - 975
(2007/10/02)

ELECTROCHEMICAL REDUCTION OF CARBON DISULFIDE. SYNTHESIS OF CARBON SULFIDE HETEROCYCLES
Detailed procedures for the electrochemical reduction of carbon disulfide in N,N-dimethylformamide and acetonitrile are given.The synthetic utility of the method is demonstrated by the preparation of several thio-substituted derivatives of tetrathiafulvalene.Cyclic voltammograms of the tetrapotassium salt of the tetrathio anion of tetrathiofulvalene indicate four successive electron-transfer steps and in situ formation of a C6S8 species.Oxidation of the CS2 electrolysis solutions produces a compound which is tentatively identified as dithiolo-1,2,3-trithiole-5-thione.
Hurley, Michael F.,Chambers, James Q.
p. 775 - 778
(2007/10/02)

Tetrathiapentalene and tetraselenapentalene compounds
This application is concerned with tetrathiapentalene and tetraselenapentalene compounds. Specifically, it is concerned with 1, 3, 4, 6-tetrathia-2, 5-dihetero-pentalene and 1, 3, 4, 6-tetraselena-2,5-dihetero-pentalene compounds having the formula STR1 w
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(2008/06/13)

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Chemical Properties

Melting Point: 182 °C (dec.)(lit.)
Boiling Point: 393 °C at 760 mmHg
Flash Point:194.7 °C
Density: 2.05 g/cm³
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C
Vapor Pressure: 2.19E-06mmHg at 25°C
Refractive Index: 1.93
PSA: 147.10000
LogP: 1.80620

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