cas 65000-12-6, 2-Bromo-N,N-diethylbenzenesulphonamide

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65000-12-6

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An approach to C-N activation: Coupling of arenesulfonyl hydrazides and arenesulfonyl chlorides with: Tert -amines via a metal-, oxidant- and halogen-free anodic oxidation
tert-Amines were harnessed to afford arenesulfonyl hydrazides and arenesulfonyl chlorides via a metal-, oxidant- and halogen-free electrochemical oxidative coupling in an undivided cell at RT. This environmentally benign approach afforded a wide spectrum of sulfonamides in satisfactory yields using cheap and renewable Pencil Graphite Electrodes (PGEs).
Sheykhan,Khani,Abbasnia,Shaabanzadeh,Joafshan
p. 5940 - 5948
(2017/12/26)

Para-Selective Alkylation of Sulfonylarenes by Cooperative Nickel/Aluminum Catalysis
A method for the para-selective alkylation of a variety of arenesulfonamides and aromatic sulfones with 1-alkenes by cooperative nickel/aluminum catalysis has been developed. Taking advantage of the sulfornyl functionality serving as a removable ortho-directing group, the reaction can be applied to facile access to 1,3-dialkyl-substitued benzenes.
Okumura, Shogo,Nakao, Yoshiaki
supporting information
p. 584 - 587
(2017/02/10)

Synthesis of sulfonamides: Via copper-catalyzed oxidative C-N bond cleavage of tertiary amines
A copper-catalyzed coupling reaction of sulfonyl chlorides with tertiary amines via the oxidative C-N bond cleavage of tertiary amines was developed. Sulfonamides were synthesized using this strategy in moderate to good yields. The reaction was applicable to various tertiary amines, as well as sulfonyl chlorides.
Ji, Jing,Liu, Zhengyi,Liu, Ping,Sun, Peipei
p. 7018 - 7023
(2016/07/30)

Catalytic conversion of aryl triazenes into aryl sulfonamides using sulfur dioxide as the sulfonyl source
Various sulfonamides have been synthesized from triazenes and sulfur dioxide. In the presence of just a catalytic amount of BF3· OEt2, a series of 1-aryl-triazenes were converted into sulfonyl hydrazines in good to excellent yields. When using CuCl2 as the catalyst, the corresponding sulfonamides can be produced from the 1-aryl triazenes in good yields. This journal is the Partner Organisations 2014.
Li, Wanfang,Beller, Matthias,Wu, Xiao-Feng
supporting information
p. 9513 - 9516
(2014/08/18)

Palladium-catalysed dehydrogenative sp3 C-H bonds functionalisation into alkenes: A direct access to N-alkenylbenzenesulfonamides
The palladium-catalysed dehydrogenation of sp3 carbon-hydrogen bonds of N-alkylbenzenesulfonamides allows a simple access to N-alkenylbenzenesulfonamides. The reaction proceeds with easily accessible catalysts, with pivalate as a base, and allo
Bheeter, Charles B.,Jin, Rongwei,Bera, Jitendra K.,Dixneuf, Pierre H.,Doucet, Henri
p. 119 - 124
(2014/03/21)

Chemical Properties

Melting Point: 76-78 °C(Solv: ethyl acetate (141-78-6); hexane (110-54-3))
Boiling Point: 365.4 °C at 760 mmHg
Flash Point:174.8 °C
Density: 1.431 g/cm³
Storage Temp.:Sealed in dry,Room Temperature
Vapor Pressure: 1.57E-05mmHg at 25°C
Refractive Index: 1.556
PKA: -5.61±0.70(Predicted)
PSA: 45.76000
LogP: 3.56040

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65000-12-6

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Chemical Properties

Melting Point: 76-78 °C(Solv: ethyl acetate (141-78-6); hexane (110-54-3))

Boiling Point: 365.4 °C at 760 mmHg

Flash Point:174.8 °C

Density: 1.431 g/cm³

Storage Temp.:Sealed in dry,Room Temperature

Vapor Pressure: 1.57E-05mmHg at 25°C

Refractive Index: 1.556

PKA: -5.61±0.70(Predicted)

PSA: 45.76000

LogP: 3.56040

Global suppliers and manufacturers of 65000-12-6total 16 suppliers on LookChem

Article Database

65000-12-6

Articles about 65000-12-6Total 5 be found

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Chemical Properties

Melting Point: 76-78 °C(Solv: ethyl acetate (141-78-6); hexane (110-54-3))

Boiling Point: 365.4 °C at 760 mmHg

Flash Point:174.8 °C

Density: 1.431 g/cm3

Storage Temp.:Sealed in dry,Room Temperature

Vapor Pressure: 1.57E-05mmHg at 25°C

Refractive Index: 1.556

PKA: -5.61±0.70(Predicted)

PSA: 45.76000

LogP: 3.56040

Global suppliers and manufacturers of 65000-12-6total 16 suppliers on LookChem

Density: 1.431 g/cm³