Protection of the carbonyl group as 1,2,4-trioxane and its regeneration under basic conditions
(Chemical Equation Presented) An experimental protocol demonstrating the protection of the carbonyl group as 1,2,4-trioxane, the stability of the protecting group under a variety of reaction conditions, and the regeneration of the carbonyl group with Triton B in THF at room temperature is presented. The method provides a useful alternative for the protection of carbonyl compounds having acid-sensitive moieties.
Singh, Chandan,Malik, Heetika
p. 5673 - 5676
(2007/10/03)
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