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Cas Database

Name	Ethyl 2-oxoheptanoate	EINECS	235-982-1
CAS No.	13078-80-3	Density	1.128 g/cm³
PSA	26.02000	LogP	2.54150
Solubility	N/A	Melting Point	145 °C
Formula	C₈H₁₀ClN	Boiling Point	239.9 °C at 760 mmHg
Molecular Weight	155.627	Flash Point	108.9 °C
Transport Information	UN 2735 8/PG 3	Appearance	Clear colorless to yellow liquid
Safety	26-36	Risk Codes	36/37/38
Molecular Structure		Hazard Symbols	Xi
Synonyms	Phenethylamine,o-chloro- (6CI,7CI,8CI);2-(2-Aminoethyl)chlorobenzene;2-(2-Chlorophenyl)ethanamine;2-(2-Chlorophenyl)ethylamine;2-Chlorobenzeneethanamine;o-Chlorophenethylamine;o-Chlorophenylethylamine;	Article Data	20

Ethyl 2-oxoheptanoate Synthetic route

: 52085-97-9
3-(2-chlorophenyl)propionyl chloride

: 13078-80-3
2-(2-chlorophenyl)ethanamine

Conditions

Conditions	Yield
With sodium azide; acetone und Erwaermen des Reaktionsprodukts in Benzol, zuletzt unter Zusatz von wss.Salzsaeure;

: 134306-93-7
3-(2-chlorophenyl)propionamide

: 13078-80-3
2-(2-chlorophenyl)ethanamine

Conditions

Conditions	Yield
With alkaline aqueous sodium hypobromite

: cyano(2-chlorophenyl)methyl ethyl carbonate

: 13078-80-3
2-(2-chlorophenyl)ethanamine

Conditions

Conditions	Yield
With hydrogenchloride; platinum Hydrogenation;

: 2856-63-5
2-Chlorophenylacetonitrile

: 13078-80-3
2-(2-chlorophenyl)ethanamine

Conditions

Conditions	Yield
With lithium aluminium tetrahydride; aluminium trichloride
With borane-THF In tetrahydrofuran at 0 - 20℃;

: 86423-60-1
Diethyl N-(2-o-chlorophenylethyl)phosphoramidate

: 13078-80-3
2-(2-chlorophenyl)ethanamine

Conditions

Conditions	Yield
With hydrogenchloride at 80 - 85℃; for 1.5h; Yield given;

: 497-25-6
dimethylenecyclourethane

: 108-90-7
chlorobenzene

A: 13078-80-3
2-(2-chlorophenyl)ethanamine

B: 156-41-2
4-chlorophenylethylamine

C CO2: CO2

Conditions

Conditions	Yield
With aluminium trichloride for 12h; Heating; 2 equivalents of AlCl3; Yield given. Title compound not separated from byproducts;

: 7647-01-0
hydrogenchloride

: cyano(2-chlorophenyl)methyl ethyl carbonate

platinum: platinum

: 13078-80-3
2-(2-chlorophenyl)ethanamine

Conditions

Conditions	Yield
Hydrogenation;

: 1-chloro-2-(2‘-nitrovinyl)benzene

: 13078-80-3
2-(2-chlorophenyl)ethanamine

Conditions

Conditions	Yield
With lithium aluminium tetrahydride In diethyl ether Heating;

: 64-04-0
phenethylamine

A: 13078-80-3
2-(2-chlorophenyl)ethanamine

B: 156-41-2
4-chlorophenylethylamine

Conditions

Conditions	Yield
With chlorine In tetrachloromethane at 25℃; Product distribution; Further Variations:; Solvents;

: 89-98-5
2-chloro-benzaldehyde

: 13078-80-3
2-(2-chlorophenyl)ethanamine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: LiAlH4 / diethyl ether / Heating View Scheme
Multi-step reaction with 2 steps 1: water 2: platinum; aq.-ethanolic hydrochloric acid / Hydrogenation View Scheme
Multi-step reaction with 2 steps 1: ammonium acetate; acetic acid / 16 h / Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C View Scheme
Multi-step reaction with 2 steps 1.1: ammonium acetate / acetic acid / 0.67 h / Heating / reflux 2.1: lithium aluminium tetrahydride; sulfuric acid / tetrahydrofuran / 0.58 h / 0 - 10 °C / Heating / reflux 2.2: 0.5 h / 20 °C View Scheme
Multi-step reaction with 2 steps 1.1: ammonium acetate; acetic acid / Neat (no solvent); Heating / reflux 2.1: aluminium hydride / tetrahydrofuran / 0.08 h / 0 °C / Heating / reflux 2.2: 0.5 h / 0 - 20 °C / Alkaline aqueous solution View Scheme

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