Tetrahedron Letters p. 6661 - 6664 (1996)
Update date:2022-08-02
Topics:
Wang, Wei
Obeyesekere, Nihal U.
McMurray, John S.
Starting from N(α)-benzyloxycarbonyl-L-tyrosine(O-triflate) benzyl ester, we have prepared enantiomerically pure 4-carboxyphenylalanine and 4-methoxycarbonylphenylalanine derivatives using palladium (0) catalyzed carbonylation reactions. These unnatural amino acids were suitably protected and were used in solid-phase peptide synthesis using the Fmoc/t-butyl approach.
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(1996)