Tetrahedron Letters p. 7975 - 7978 (1998)
Update date:2022-08-05
Topics:
Vyle, Joseph S.
Williams, Nicholas H.
Grasby, Jane A.
Michaelis-Arbusov chemistry was used to prepare O,S-dialkyl 3'-O- nucleosidyl phosphorothiolate triesters in solution and attached to CPG. The support-bound nucleoside was utilised in the synthesis of a pentaribonucleotide that was fully deprotected on the support. Subsequent treatment with a buffered solution of iodine cleaved the RNA from the CPG with concomitant formation of a terminal 2',3'-cyclic phosphate.
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