Synthesis p. 760 - 761 (1986)
Update date:2022-08-02
Topics:
Martinez, Manuel A.
Vega, Juan C.
The preparation of O-alkyl carbonochloridothioates (2) was improved by performing the reaction of thiophosgene with potassium alkoxides in the corresponding alcohol or in tetrahydrofuran at -65 deg C for 1 hour.In all cases, the reaction yielded products 2, O,O-dialkyl carbonothioates (4), and dialkyl carbonates (5) in varying distribution.
View MoreChangzhou LanXu Chemical Co.,ltd.
Contact:86-0519-86330911,13656129734,15261186386
Address:Room 524, Depart.Chemical, Changzhou Science and Eductaion town, Jiangsu, China;Factory: Haian Fine Chemical Industry Park,Nantong,Jiangsu,China
Contact:18669908765
Address:Zibo City, Shandong Province, P.R.China
NINGBO PANGS CHEM INT’L CO., LTD.
Contact:+86-0574-27666801
Address:Floor 21, Building 11, Xintiandi, No. 689, Shijiroad, Ningbo, Zhejiang, China
Contact:+1-416-493-6870
Address:Toronto, Canada
Buffett (China) Holding Co.,Ltd
Contact:4006570891
Address:
Doi:10.1021/acs.orglett.7b01047
(2017)Doi:10.1016/0031-9422(88)80449-7
(1988)Doi:10.1016/j.tet.2014.10.077
(2014)Doi:10.1016/S0040-4039(00)82032-8
(1988)Doi:10.1055/s-1988-27521
(1988)Doi:10.1016/j.saa.2009.01.019
(2009)