Synthetic Communications p. 15 - 20 (1995)
Update date:2022-09-26
Topics:
Black
Zhang
Huang
Smith
Yates
Saturated and unsaturated aldehydes and ketones, when treated with trimethylsilylketene and BF3 for 16 hours, form β-lactones which spontaneously rearrange to α,β-unsaturated TMS esters; these hydrolyze during workup to form the corresponding carboxylic acids.
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