Synthetic Communications p. 3503 - 3508 (1998)
Update date:2022-08-11
Topics:
Mo, Zunli
Yang, Wu
Gao, Jinzhang
Chen, Hong
Gong, Qiaojuan
Hou, Jingguo
Kang, Jingwan
A new two-step synthesis method of macrobicyclic hexaamide ligands LH6 (I and II) with double condensation of triethyl nitrilotriacetate and 1,4(1,2)-diaminobenzene was developed. The cyclization does not require high dilution and template techniques. Two new hexaamide ligands were prepared in good yields according to the proposed method.
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