Carbohydrate Research p. 1195 - 1199 (2004)
Update date:2022-08-11
Topics:
Dabrowska, Aleksandra
Sikorski, Artur
Jacewicz, Dagmara
Chmurzynski, Lech
The structure, conformation and configuration of methyl 3-amino-2,3-dideoxy-α-D-arabino-hexopyranoside (I) were confirmed by 1H NMR, 13C NMR and IR spectroscopy, as well as by optical rotation. The structure of the compound studied was also determined by single crystal X-ray crystallography at 293K and refined to a final R=0.0521 based on 1798 independent reflections. The title compound crystallized in the tetragonal space group P43 with a=6.572(1)A, b=6.572(1)A, c=41.161(8)A, Dc=1.324Mgcm-3 and V=1777.8(5)A3 for Z=8. The packing arrangement in the unit cell displayed a stratified structure. Moreover, medium-strength N-H...O and O-H...O hydrogen bonds, which stabilized the 3-D structure of compound I, were observed.
View Morewebsite:http://www.afinechem.com
Contact:+86-571-85134551
Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China
Dalian Synco Chemical Co., Ltd.
Contact:+86-411-83635150
Address:Rm 1004, 24, Tangshan Street, Dalian
Contact:+86-913-2223392
Address:No. 32, Xinanjing Road, Weinan City, Shaanxi Province, 714000, China
Nanjing Chemzam Pharmtech Co., Ltd.
Contact:+86-25-86462165,+86-13915979898
Address:C5-1,6 Maiyue Road,Maigaoqiao,Nanjing,Jiangsu,China
Lyrin Industrial Corporation Limited
Contact:86-731-82571800
Address:Rm 2408,Asia Economy International Building,Shaoshan Road South,Yuhua District,Changsha,Hunan,China
Doi:10.1002/adsc.201500378
(2015)Doi:10.1002/hlca.19560390637
(1956)Doi:10.1016/j.abb.2018.07.005
(2018)Doi:10.1246/cl.1980.977
(1980)Doi:10.1016/S0040-4020(01)91327-4
(1984)Doi:10.1039/c4cc05433d
(2014)