Turkish Journal of Chemistry p. 1706 - 1719 (2018)
Update date:2022-08-11
Topics:
Yilmaz, ülkü
Kü?ükbay, Hasan
Many benzimidazole salts bearing a 3-phenylpropyl substituent (1a–1h) were synthesized and their structures were identified by1 H NMR,13 C NMR, and IR spectroscopic methods and elemental analysis. These N-heterocyclic carbene (NHC) precursors were used as a part of a catalytic system including Pd(OAc) 2 and the base in the Suzuki–Miyaura cross-coupling reaction under microwave irradiation. They were also used as catalysts in the cyclotrimerization of phenyl isocyanate to yield 1,3,5-triphenyl-1,3,5-triazinane-2,4,6-trione. It has been observed that benzimidazole salts made a positive contribution to both catalytic reactions as a NHC precursor.
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