Journal of Organometallic Chemistry p. 611 - 613 (1997)
Update date:2022-08-30
Topics:
Kunai, Atsutaka
Mihara, Toshiyuki
Matsuo, Yoichi
Ohshita, Joji
Naka, Akinobu
Ishikawa, Mitsuo
The cothermolysis of 1,1-dimesityl-3-phenyl-2-trimethylsilyl-1-silacyclopropene (1) with 1,4-bis(triethylsilyl)- and 1,4-bis(triethylsilyl)butadiyne at 250°C for 24 h afforded 1,1-dimesityl-3-silyl-2-silylethynyl-1-silacyclopropenes (3 and 5) and dimesitylbis(silylethynyl)silanes (4 and 6), respectively. The thermolysis of silacyclopropene 3 under the same conditions cleanly produced an isomerization product 4.
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