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Name	Methoxypropiophenone	EINECS	204-512-7
CAS No.	121-97-1	Density	1.071 g/cm³
PSA	26.30000	LogP	2.28790
Solubility	N/A	Melting Point	27-29 °C(lit.)
Formula	C₁₀H₁₂O₂	Boiling Point	272.316 °C at 760 mmHg
Molecular Weight	164.204	Flash Point	118.806 °C
Transport Information	UN 1993	Appearance	Clear colourless to amber liquid
Safety	24/25	Risk Codes	N/A
Molecular Structure		Hazard Symbols	Xi
Synonyms	p-Methoxypropiophenone;4-Methoxypropiophenone;Propiophenone,4'-methoxy- (6CI,7CI,8CI);Propiophenone, p-methoxy- (4CI);1-(4-Methoxyphenyl)-1-propanone;1-Methoxy-4-propanoylbenzene;4-Propanoylanisole;4'-Methoxypropiophenone;Ethyl 4-methoxyphenyl ketone;Ethyl p-methoxyphenyl ketone;NSC 11834;	Article Data	223

Methoxypropiophenone Synthetic route

: 79-03-8
propionyl chloride

: 100-66-3
methoxybenzene

: 121-97-1
4-Methoxypropiophenone

Conditions

Conditions	Yield
With Noccaea caerulescens extract supported in montmorillonite K10 at 60℃; for 6h; Friedel Crafts acylation; Inert atmosphere; regioselective reaction;	100%
With aluminum (III) chloride In dichloromethane at 5 - 20℃; for 2.5h;	98%
With benzyltributylammonium tetrachloroferrate at 50℃; for 0.1h; Friedel-Crafts reaction;	93%

: 100-66-3
methoxybenzene

: 123-62-6
propionic acid anhydride

: 121-97-1
4-Methoxypropiophenone

Conditions

Conditions	Yield
With lithium perchlorate at 60℃; for 1h;	99%
Stage #1: methoxybenzene; propionic acid anhydride With modified ZSM-5 zeolite at 100℃; for 5h; Stage #2: at 500℃; for 2h; Temperature; Calcination;	97.6%
With hafnium(IV) trifluoromethanesulfonate; lithium perchlorate In nitromethane for 6h; Ambient temperature;	93%

: 51410-44-7
1-(4-methoxylphenyl)-2-propen-1-ol

: 121-97-1
4-Methoxypropiophenone

Conditions

Conditions	Yield
With tris(acetonitrile)pentamethylcyclopentadienylruthenium(II) hexafluorophosphate; potassium carbonate In acetonitrile for 1h; Inert atmosphere; Reflux;	99%
With [Ru(η(3):η(3)-C10H16)Cl(O2CCH3)] In aq. phosphate buffer at 50℃; for 1h; pH=7; Sealed tube; Inert atmosphere;	99%
With Fe(II)(bis(2-(diisopropylphosphino)ethyl)amine)(CO)(H)(Cl); potassium tert-butylate In toluene at 80℃; for 1h; Inert atmosphere;	98%

: 97-94-9
triethyl borane

: 4-methoxy-N-phenyl-N-tosylbenzamide

: 121-97-1
4-Methoxypropiophenone

Conditions

Conditions	Yield
With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; potassium carbonate In tetrahydrofuran; tert-butyl methyl ether at 20℃; for 24h; Inert atmosphere; Schlenk technique;	99%

: 75-57-0
tetramethlyammonium chloride

: 70-70-2
4-hydroxypropiophenone

: 121-97-1
4-Methoxypropiophenone

Conditions

Conditions	Yield
With potassium carbonate In 1,2-dimethoxyethane at 145℃; for 0.416667h; Microwave irradiation; Inert atmosphere; Sealed vessel;	98%
With potassium carbonate at 150 - 160℃; for 4h;	81%

: 92409-14-8
C17H20O4

: 121-97-1
4-Methoxypropiophenone

Conditions

Conditions	Yield
With 5%-palladium/activated carbon; ammonium formate In ethanol; water at 80℃; for 1h;	98%

: 5349-60-0
1-(4-methoxyphenyl)-1-propanol

A: 623-12-1
4-chloromethoxybenzene

B: 121-97-1
4-Methoxypropiophenone

Conditions

Conditions	Yield
With dichloromethane extract derived from 6percent aqueous hypochlorite/tetra-n-butylammonium bisulfate solution with pH value to 8-9 In dichloromethane at 20℃;	A 92% B 6%

: 77-78-1
dimethyl sulfate

: 70-70-2
4-hydroxypropiophenone

: 121-97-1
4-Methoxypropiophenone

Conditions

Conditions	Yield
With potassium carbonate In acetonitrile for 20.5h; Heating / reflux;	89%
With sodium hydroxide
With hydroxide

: 94607-41-7
(E)-1-(4-methoxyphenyl)-3-chloropropene

: 121-97-1
4-Methoxypropiophenone

Conditions

Conditions	Yield
With potassium carbonate; phenylboronic acid; [Ru(cyclopentadienyl)(MeCN)3]PF6 In acetonitrile at 20℃; for 16h;	89%
With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; potassium carbonate; phenylboronic acid In acetonitrile at 20℃; for 24h; Inert atmosphere; regioselective reaction;	89%

: 52898-49-4
4,N-dimethoxy-N-methylbenzamide

: 925-90-6
ethylmagnesium bromide

: 121-97-1
4-Methoxypropiophenone

Conditions

Conditions	Yield
In tetrahydrofuran at 0 - 5℃; for 1h; Weinreb Ketone Synthesis; Inert atmosphere;	89%

Methoxypropiophenone Chemical Properties

IUPAC Name: 1-(4-Methoxyphenyl)propan-1-one
Systematic of 1-Propanone,1-(4-methoxyphenyl)- (CAS NO.121-97-1): 4'-Methoxypropiophenone ; AI3-04094 ; EINECS 204-512-7 ; Ethyl 4-methoxyphenyl ketone ; NSC 11834 ; p-Methoxypropiophenone ; Propiophenone, 4'-methoxy- (8CI)
CAS NO: 121-97-1
Molecular Formula of 1-Propanone,1-(4-methoxyphenyl)- (CAS NO.121-97-1): C₁₀H₁₂O₂
Molecular Weight: 164.2011
Molecular Structure:

Melting Point: 27-29 °C
H bond acceptors: 2
Freely Rotating Bonds: 3
Polar Surface Area: 26.3 Å²
Index of Refraction: 1.501
Molar Refractivity: 47.59 cm³
Molar Volume: 161.4 cm³
Surface Tension: 33.6 dyne/cm
Density of 1-Propanone,1-(4-methoxyphenyl)- (CAS NO.121-97-1): 1.016 g/cm³
Flash Point: 118.8 °C
Enthalpy of Vaporization: 51.06 kJ/mol
Boiling Point: 272.3 °C at 760 mmHg
Vapour Pressure: 0.00612 mmHg at 25°C

Methoxypropiophenone Safety Profile

Hazard Codes: Xi
Safety Statements: 24/25
S24/25: Avoid contact with skin and eyes.
RIDADR: 1993
WGK Germany: 3
Hazard Note: Irritant

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