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Cas Database

Name	N-Nitromethylamine	EINECS	N/A
CAS No.	598-57-2	Density	1.236g/cm³
PSA	57.85000	LogP	0.31160
Solubility	N/A	Melting Point	38°C
Formula	CH4 N2 O2	Boiling Point	155.2°Cat760mmHg
Molecular Weight	76.055	Flash Point	47.6°C
Transport Information	N/A	Appearance	N/A
Safety	Moderately toxic by intraperitoneal route. Questionable carcinogen with carcinogenic data. Mutation data reported. Explodes on contact with concentrated sulfuric acid. When heated to decomposition it emits toxic fumes of NO_x. See also NITRO COMPOUNDS and AMINES.	Risk Codes	N/A
Molecular Structure		Hazard Symbols	N/A
Synonyms	Methylamine,N-nitro- (6CI,7CI,8CI); Methylnitramine; Methylnitroamine; N-Methylnitramine;N-Nitromethylamine; NSC 137855	Article Data	26

N-Nitromethylamine Synthetic route

: 96-31-1
N,N'-Dimethylurea

: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
Stage #1: N,N'-Dimethylurea With sulfuric acid; nitric acid In dichloromethane at -5 - 0℃; Stage #2: In water at 20℃; for 1h; Temperature;	89.2%

: 141-52-6
sodium ethanolate

: 99647-88-8
1-phenyl-3-(methylnitroamino)-2-propen-1-one

A: 36234-10-3
3-Oxo-3-phenylpropanal 1-(diethylacetal)

B: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
In ethanol at 35 - 40℃; for 3h;	A 65% B n/a

: 186581-53-3, 908094-01-9
diazomethane

: 556-89-8
nitrourea

: 598-57-2
methylnitroamine

: 186581-53-3, 908094-01-9
diazomethane

: N-nitro-N'-ethyl-urea

A: 598-57-2
methylnitroamine

B: 4164-28-7
N-nitrodimethylamine

C: 109-90-0
ethyl isocyanate

: 687-48-9
ethyl N,N-dimethylcarbamate

: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
With nitric acid nimmt das erhaltene Nitromethylurethan mit Aether auf und leitet in die aether. Loesung trocknes NH3 ein;

: 14442-54-7
methyl-nitro-carbamic acid methyl ester

: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
With diethyl ether; ammonia der Entstandene Niederschlag des Ammoniumsalzes mit Aether gewaschen und durch Kochen mit Alkohol zersetzt wird;

: 91086-49-6
bis-(N-methyl-N-ethoxycarbonylamino)methane

: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
With nitric acid at -8℃; Leiten von NH3 in die aether.Loesung des Reaktionsprodukts;

: 14760-99-7
N,N’-dimethyl-N,N’-dinitrooxalamide

: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
With ammonium hydroxide Entsteht als Ammoniumsalz;
With barium dihydroxide; water man faellt freien Baryt durch CO2, dammpft die Loesung ein, versetzt den Rueckstand mit der theoretischen Menge Schwefelsaeure und nimmt das freie Methylnitramin in Aether auf;
With ammonia at 5 - 20℃; under 6000.6 Torr; for 0.333333h; Autoclave;	0.61 g

: 60-29-7
diethyl ether

: N-methyl-N-nitro-N'-phenyl-urea

: 62-53-3
aniline

A: 598-57-2
methylnitroamine

B: 603-54-3
N,N-diphenylurea

: 598-50-5
N-Methylurea

: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
Nitrierung von Methylharnstoff und letzterer zerfaellt bei der Aufarbeitung des Reaktionsprodukts durch Behandeln mit Ammoniak;

N-Nitromethylamine Chemical Properties

IUPAC Name: Nitromethanamine
Synonyms of N-Nitromethylamine (CAS NO.598-57-2) : Methanamine, N-nitro- (9CI) ; Methyl nitramine (dry) [Forbidden] ; Nitramine, methyl-
InChI:InChI=1/CH4N2O2/c2-1-3(4)5/h1-2H2
CAS NO:598-57-2
Molecular Formula:CH₄N₂O₂
Molecular Weight :76.0547
Molecular Structure :
Index of Refraction: 1.44
Surface Tension: 45.2 dyne/cm
Density: 1.236 g/cm³
Flash Point: 47.6 °C
Enthalpy of Vaporization: 39.19 kJ/mol
Boiling Point: 155.2 °C at 760 mmHg
Vapour Pressure: 3.07 mmHg at 25°C

N-Nitromethylamine Toxicity Data With Reference

Organism	Test Type	Route	Reported Dose (Normalized Dose)	Effect	Source
mouse	LD50	intraperitoneal	500mg/kg (500mg/kg)		Pharmaceutical Chemistry Journal Vol. 10, Pg. 1504, 1976.

N-Nitromethylamine Safety Profile

N-Nitromethylamine (CAS NO.598-57-2) is moderately toxic by intraperitoneal route. Questionable carcinogen with carcinogenic data. Mutation data reported. Explodes on contact with concentrated sulfuric acid. When N-Nitromethylamine (CAS NO.598-57-2) is heated to decomposition ,it emits toxic fumes of NO_x. See also NITRO COMPOUNDS and AMINES.

N-Nitromethylamine Standards and Recommendations

DOT Classification: Forbidden

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