5-Quinolinethiol

Base Information

• Chemical Name: 5-Quinolinethiol
• CAS No.: 3056-03-9
• Molecular Formula: C9H7NS
• Molecular Weight: 161.227
• Mol file: 3056-03-9.mol

Synonyms:

Chemical Property of 5-Quinolinethiol

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Quinolinethiol

There total 1 articles about 5-Quinolinethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-bromoquinoline (4964-71-0) → 5-mercaptoquinoline (3056-03-9)

Guidance literature:

With sodium thiomethoxide; In N,N-dimethyl-formamide; for 4h; Heating;

DOI:10.3987/COM-07-11088

Reference yield: 86.0%

5-mercaptoquinoline (3056-03-9) → quinoline-5-sulfonyl chloride (102878-84-2)

Guidance literature:

With chlorine; In water; acetic acid; at 15 - 17 ℃; for 0.5h;

DOI:10.3987/COM-07-11088

Reference yield: 47.0%

5-mercaptoquinoline (3056-03-9) + 3-Phenyl-2-propynonitrile (935-02-4) → (Z)-3-Phenyl-3-(quinolin-5-ylsulfanyl)-acrylonitrile

Guidance literature:

With potassium hydroxide; In 1,4-dioxane; at 40 - 50 ℃; for 25h;

upstream raw materials:

5-bromoquinoline

Downstream raw materials:

thiobenzoic acid S-[5]quinolyl ester

Z-5-styrylthioquinoline

quinoline-5-sulfonyl chloride

5-benzoylmercapto-1-methyl-quinolinium; iodide

Refernces