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3-Amino-6-chloro-2-picoline

Base Information Edit
  • Chemical Name:3-Amino-6-chloro-2-picoline
  • CAS No.:164666-68-6
  • Molecular Formula:C6H7ClN2
  • Molecular Weight:142.59
  • Hs Code.:29333990
  • European Community (EC) Number:676-221-7
  • DSSTox Substance ID:DTXSID50426559
  • Wikidata:Q72434781
  • Mol file:164666-68-6.mol
3-Amino-6-chloro-2-picoline

Synonyms:164666-68-6;3-Amino-6-chloro-2-picoline;6-chloro-2-methylpyridin-3-amine;3-amino-6-chloro-2-methylpyridine;5-amino-2-chloro-6-methylpyridine;6-CHLORO-2-METHYL-PYRIDIN-3-YLAMINE;3-PYRIDINAMINE, 6-CHLORO-2-METHYL-;MFCD03095220;5-amino-2-chloro-6-picoline;2-CHLORO-5-AMINO-6-METHYLPYRIDINE;SCHEMBL1128266;DTXSID50426559;QVCIIOZINFCMDJ-UHFFFAOYSA-N;BCP22075;CS-D0972;3-amino-6-chloro-2-methyl pyridine;AKOS005257276;AC-5421;PB20018;6-CHLORO-2-METHYL-3-PYRIDINAMINE;AS-14933;SY007925;3-amino-6-chloro-2-picoline, AldrichCPR;AM20050863;FT-0648987;EN300-181110;Q-103404

Suppliers and Price of 3-Amino-6-chloro-2-picoline
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • TRC
  • 6-Chloro-2-methylpyridin-3-amine
  • 10g
  • $ 470.00
  • SynQuest Laboratories
  • 6-Chloro-2-methylpyridin-3-amine
  • 5 g
  • $ 95.00
  • Matrix Scientific
  • 5-Amino-2-chloro-6-methylpyridine 98%
  • 25g
  • $ 136.00
  • Matrix Scientific
  • 5-Amino-2-chloro-6-methylpyridine 98%
  • 1g
  • $ 10.00
  • Matrix Scientific
  • 5-Amino-2-chloro-6-methylpyridine 98%
  • 5g
  • $ 44.00
  • Frontier Specialty Chemicals
  • 3-Amino-6-chloro-2-picoline 97%
  • 1g
  • $ 35.00
  • Frontier Specialty Chemicals
  • 3-Amino-6-chloro-2-picoline 97%
  • 5g
  • $ 129.00
  • Crysdot
  • 6-Chloro-2-methylpyridin-3-amine 98%
  • 100g
  • $ 189.00
  • Chemenu
  • 6-chloro-2-methylpyridin-3-amine 98%
  • 100g
  • $ 256.00
  • Chemcia Scientific
  • 6-Chloro-2-methyl-pyridin-3-ylamine 97%
  • 25 G
  • $ 125.00
Total 100 raw suppliers
Chemical Property of 3-Amino-6-chloro-2-picoline Edit
Chemical Property:
  • Vapor Pressure:0.00272mmHg at 25°C 
  • Melting Point:93-94℃ 
  • Refractive Index:1.592 
  • Boiling Point:286 °C at 760 mmHg 
  • PKA:1.79±0.10(Predicted) 
  • Flash Point:126.7 °C 
  • PSA:38.91000 
  • Density:1.26 g/cm3 
  • LogP:2.20680 
  • Storage Temp.:Keep in dark place,Inert atmosphere,Store in freezer, under -20°C 
  • XLogP3:1.5
  • Hydrogen Bond Donor Count:1
  • Hydrogen Bond Acceptor Count:2
  • Rotatable Bond Count:0
  • Exact Mass:142.0297759
  • Heavy Atom Count:9
  • Complexity:97.1
Purity/Quality:

99% *data from raw suppliers

6-Chloro-2-methylpyridin-3-amine *data from reagent suppliers

Safty Information:
  • Pictogram(s): IrritantXi,Toxic
  • Hazard Codes:Xi,T,Xn 
  • Statements: 22-37/38-41-20/21/22 
  • Safety Statements: 26-39-36/37-24/25 
MSDS Files:

SDS file from LookChem

Useful:
  • Canonical SMILES:CC1=C(C=CC(=N1)Cl)N
  • Uses 6-Chloro-2-methylpyridin-3-amine has been used as a reactant in the preparation of Pyrido[3,2-e][1,4]diazepine derivatives with anti-HIV-1-activity.
Technology Process of 3-Amino-6-chloro-2-picoline

There total 6 articles about 3-Amino-6-chloro-2-picoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With trifluoroacetic acid; In dichloromethane; for 2h; Reflux;
Guidance literature:
With hydrogenchloride; iron; In ethanol; water; at 20 ℃; for 1h;
Guidance literature:
Multi-step reaction with 4 steps
1: liquid NH3; xylene; Fe(NO3)3
2: concentrated H2SO4; concentrated HNO3
3: sodium nitrite; concentrated aqueous hydrochloric acid / Diazotization
4: SnCl2; concentrated aqueous HCl
With hydrogenchloride; sulfuric acid; ammonia; nitric acid; ferric nitrate; tin(ll) chloride; xylene; sodium nitrite;
DOI:10.1021/ja01193a016
Refernces Edit
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