1-NITROPERYLENE

Base Information

• Chemical Name: 1-NITROPERYLENE
• CAS No.: 35337-20-3
• Molecular Formula: C20H11NO2
• Molecular Weight: 297.313
• Hs Code.: 2904209090
• Mol file: 35337-20-3.mol

Synonyms:1-Nitroperylen;1-nitroperilene;1-pentylnitrate;Pentane,1-nitro;1-nitro-pentane;1-Nitro-pentan;amyl nitrite;1-nitropenthane;

Chemical Property of 1-NITROPERYLENE

Chemical Property:

• Vapor Pressure: 6.33E-11mmHg at 25°C
• Melting Point: 210 °C(Solv: benzene (71-43-2); cyclohexane (110-82-7))
• Boiling Point: 533.5oC at 760 mmHg
• Flash Point: 265.4oC
• PSA: 45.82000
• Density: 1.429g/cm3
• LogP: 4.57720

Purity/Quality:

99% ^*data from raw suppliers

1-NITROPERYLENE 98.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-NITROPERYLENE

There total 5 articles about 1-NITROPERYLENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

PERYLENE (198-55-0) → 3-Nitroperylene (20589-63-3) + 1-nitroperilene (35337-20-3)

Guidance literature:

With nitric acid; In 1,4-dioxane; at 60 - 80 ℃; for 0.5h;

Reference yield: 43.3%

PERYLENE (198-55-0) → 1-nitroperilene (35337-20-3)

Guidance literature:

With nitric acid; In 1,4-dioxane; water; at 70 - 95 ℃; for 1h;

Reference yield: 26.0%

3-Nitroperylene (20589-63-3) → 1-nitroperilene (35337-20-3)

Guidance literature:

With methanesulfonic acid; In triethyl phosphite;

upstream raw materials:

PERYLENE

3-Nitroperylene

Downstream raw materials:

diethyl 7-nitrobenzo[g,h,i]perylene-1,2-dicarboxylate

perilo[1,12-b,c,d]thiophene

1-hydrophenanthrene[1,10,9,8-cdefg]carbazole

perilo[1,12-b,c,d]selenophene

Refernces

• 1、 Santoni, Marie-Pierre,Santoro, Antonio,Salerno, Tania M. G.,Puntoriero, Fausto,Nastasi, Francesco,Di Pietro, M. Letizia,Galletta, Maurilio,Campagna, Sebastiano. "Photoinduced Charge Separation in a Donor-Spacer-Acceptor Dyad with N-Annulated Perylene Donor and Methylviologen Acceptor". . p. 3147 - 3150. Retrieved 2015.
• 2、 Looker,J.J.. "-". . p. 3379 - 3381. Retrieved 1972.
• 3、 Elmali, Ayhan,Hu, Mengyu,Ji, Shaomin,Karatay, Ahmet,Sukhanov, Andrei A.,Voronkova, Violeta K.,Zhang, Xue,Zhao, Jianzhang. "Spiro Rhodamine-Perylene Compact Electron Donor-Acceptor Dyads: Conformation Restriction, Charge Separation, and Spin-Orbit Charge Transfer Intersystem Crossing". . p. 4187 - 4203. Retrieved 2021/05/31.
• 4、 -. "A kind of star-shaped fluorescent molecule and its preparation method and application (by machine translation)". Paragraph 0053-0055. . Retrieved 2019/01/08.