Ethanimidoyl fluoride, 2,2,2-trifluoro-N-(pentafluoroethyl)-

Base Information

• Chemical Name: Ethanimidoyl fluoride, 2,2,2-trifluoro-N-(pentafluoroethyl)-
• CAS No.: 380-66-5
• Molecular Formula: C4F9N
• Molecular Weight: 233.036
• Mol file: 380-66-5.mol

Synonyms:

Chemical Property of Ethanimidoyl fluoride, 2,2,2-trifluoro-N-(pentafluoroethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanimidoyl fluoride, 2,2,2-trifluoro-N-(pentafluoroethyl)-

There total 3 articles about Ethanimidoyl fluoride, 2,2,2-trifluoro-N-(pentafluoroethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethylamine (109-89-7) → Hexafluoroethane (76-16-4) + pentafluoroethyl-tetrafluoroethyliden-amine (380-66-5) + N-Fluor-perfluordiaethylamin (815-29-2)

Guidance literature:

With hydrogen fluoride; at 7 - 8 ℃; for 8.16667h; Title compound not separated from byproducts; Electrolysis;

DOI:10.1016/S0022-1139(00)00267-0

Reference yield:

perfluoro(N,N-diethylcarbamoyl fluoride) (105968-23-8) → Carbonyl fluoride (353-50-4) + pentafluoroethyl-tetrafluoroethyliden-amine (380-66-5)

Guidance literature:

With lithium dimethylamide; at -196 - 20 ℃; for 19h;

DOI:10.1016/S0022-1139(00)84155-X

Reference yield:

N,N-diperfluorodiethyl-N-(2-hydroperfluoro-2-methylpentyl)amine (89810-76-4) → pentafluoroethyl-tetrafluoroethyliden-amine (380-66-5) + perfluoro-2-methylpent-2-ene (1584-03-8) + 1,1,1,2,2,3,3,5,5,5-decafluoro-4-trifluoromethyl-pentane (30320-28-6)

Guidance literature:

With triethylamine; at 100 ℃; for 3h;

DOI:10.1007/BF00954714

upstream raw materials:

N,N-diperfluorodiethyl-N-(2-hydroperfluoro-2-methylpentyl)amine

perfluoro(N,N-diethylcarbamoyl fluoride)

diethylamine

Downstream raw materials:

carbon dioxide

ammonia

sodium 2,2,2-trifluoroacetate

sodium fluoride

Refernces

• 1、 Abe, Takashi,Hayashi, Eiji. "THE SYNTHESIS OF PERFLUORO(N,N-DIALKYLCARBAMOYL FLUORIDES) BY THE REACTION OF PERFLUORO(N,N-DIALKYLMETHYLAMINES) WITH OLEUM". . p. 293 - 312. Retrieved 2007/10/02.