Tri(ethylamino)borane

Base Information

• Chemical Name: Tri(ethylamino)borane
• CAS No.: 4254-92-6
• Molecular Formula: C6H18BN3
• Molecular Weight: 143.04
• Mol file: 4254-92-6.mol

Synonyms:Tris-(ethylamino)-boran;tris-ethylamino-borane;Tris-aethylamino-boran;Tris-[ethylamino]-boran;Borsaeure-tris-ethylamid;Tris-aethylamino-borin;

Chemical Property of Tri(ethylamino)borane

Chemical Property:

• PSA: 36.09000
• LogP: 0.97250

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tri(ethylamino)borane

There total 9 articles about Tri(ethylamino)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

boron trichloride (10294-34-5) + ethylamine (75-04-7,85404-22-4) → tris(ethylamino) borane (4254-92-6)

Guidance literature:

In pentane; -80°C;

Reference yield:

ethylamine (75-04-7,85404-22-4) → tris(ethylamino) borane (4254-92-6)

Guidance literature:

With lithium;

DOI:10.1021/ja01374a034

Reference yield:

boron trifluoride (7637-07-2) + lithium (7439-93-2) + ethylamine (75-04-7,85404-22-4) → tris(ethylamino) borane (4254-92-6) + lithium fluoride (7789-24-4)

Guidance literature:

In ammonia; byproducts: H2;

DOI:10.1021/ja01374a034

upstream raw materials:

ethylamine

boron trifluoride

lithium

boron trichloride

Downstream raw materials:

B-tris(ethylamino)-N-triethylborazine

ethylamine

Refernces

• 1、 Melcher,Boenig,Niedenzu. "Preparation of ethylamine-borane by electrolysis of sodium tetrahydridoborate in ethylamine". . p. 487 - 488. Retrieved 2007/10/05.