D-Lysine methyl ester

Base Information

• Chemical Name: D-Lysine methyl ester
• CAS No.: 42807-32-9
• Molecular Formula: C₇H₁₆N₂O₂
• Molecular Weight: 160.216
• Mol file: 42807-32-9.mol

Synonyms:D-LYSINE METHYL ESTER;Lysine Methyl Ester;lysine diester;DL-Lys-OCH3;rac-Lysin-methylester;

Chemical Property of D-Lysine methyl ester

Chemical Property:

• PSA: 78.34000
• LogP: 1.01630

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of D-Lysine methyl ester

There total 7 articles about D-Lysine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.8%

2C7H16N2O2*H2O4S → DL-lysine methyl ester (687-64-9,42807-32-9,44977-95-9)

Guidance literature:

With ammonium hydroxide; In water; at 5 - 20 ℃; pH=8-9;

Reference yield: 93.0%

methanol (67-56-1) + D-lysine (923-27-3,3506-25-0) → D-lysine methyl ester (687-64-9,42807-32-9,44977-95-9)

Guidance literature:

With hydrogenchloride; 2,2-dimethoxy-propane;

DOI:10.1002/chem.200400502

Reference yield:

methanol (67-56-1) + 2,6-diaminocaproic acid (70-54-2,923-27-3,6899-06-5,60103-30-2,60132-27-6,56-87-1,3506-25-0) → DL-lysine methyl ester (687-64-9,42807-32-9,44977-95-9)

Guidance literature:

With acetyl chloride; at 70 ℃; for 1h;

DOI:10.1002/rcm.5174

upstream raw materials:

methanol

Lysin-dihydrochlorid

2,6-diaminocaproic acid

D-lysine

Downstream raw materials:

N^α,N^ε-bis<(R)-α-methylbenzylcarbamoyl>-DL-lysine methyl ester

(2S,1'R)-N⁶-<1-(Ethoxycarbonyl)ethyl>lysin-methylester

(2R,1'R)-N⁶-<1-(Ethoxycarbonyl)ethyl>lysin-methylester

Ac-D-F-D-K

Refernces

• 1、 -. "Preparation and application of guaifenazulene aldole dicondensate (by machine translation)". Paragraph 0019; 0020. . Retrieved 2019/08/02.
• 2、 Lee, Yen Jea,Kang, Boyeong,Seo, Jiwon. "Metalloporphyrin dimers bridged by a peptoid helix: Host-guest interaction and chiral recognition". . . Retrieved 2018/11/03.