Tris(p-fluorophenyl)borane

Base Information Edit

Chemical Name:Tris(p-fluorophenyl)borane
CAS No.:47196-74-7
Molecular Formula:C18H12BF3
Molecular Weight:296.099
Hs Code.:
Mol file:47196-74-7.mol

Synonyms:(4FC6H4)3B;B(4-F2C6H3)3;Tris-(4-fluoro-phenyl)-borane;tris(p-fluorophenyl)borane;

Suppliers and Price of Tris(p-fluorophenyl)borane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Tris(p-fluorophenyl)borane Edit

Chemical Property:

PSA：0.00000
LogP:2.62010

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Tris(p-fluorophenyl)borane

There total 13 articles about Tris(p-fluorophenyl)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 353-42-4
boron trifluoride dimethyl etherate

: 460-00-4
1-Bromo-4-fluorobenzene

: 47196-74-7
tris(4-fluorophenyl)borane

Guidance literature:: With magnesium; In diethyl ether; toluene; react. of 50mmol 4-FC6H4Br in 20ml ether with 50mmol Mg in 30ml ether at 0°C, stirring for 5h, dropwise addn. of the soln. to 17mmol BF3*OMe2 in 50ml toluene at -20°C;; distn. of ether; removal of Mg-salts by filtration; distn. of toluene; recrystn. of residue from pentane; detn. by (13)C-, (19)F-, (1)H-NMR, mass spectroscopy;;