1,3-Bis(3-aminophenoxy)benzene

Base Information

• Chemical Name: 1,3-Bis(3-aminophenoxy)benzene
• CAS No.: 10526-07-5
• Molecular Formula: C18H16N2O2
• Molecular Weight: 292.337
• Hs Code.: 29222990
• European Community (EC) Number: 234-082-6
• DSSTox Substance ID: DTXSID4065109
• Nikkaji Number: J105.954H
• Wikidata: Q72444103
• Mol file: 10526-07-5.mol

Synonyms:1,3-Bis(3-aminophenoxy)benzene;10526-07-5;3,3'-(1,3-Phenylenebis(oxy))dianiline;3-[3-(3-aminophenoxy)phenoxy]aniline;Benzenamine, 3,3'-[1,3-phenylenebis(oxy)]bis-;1,3-bis-(3-Aminophenoxy)benzene;Resorcinol Bis(3-aminophenyl) Ether;3,3'-(m-Phenylenedioxy)dianiline;EINECS 234-082-6;MFCD00043718;3,3'-(1,3-Phenylenedioxy)dianiline-15N2;Benzenamine, 3,3'-(1,3-phenylenebis(oxy))bis-;3,3'-(m-Phenylenebis(oxy))dianiline;3,3'-[m-phenylenebis(oxy)]dianiline;3,3'-[1,3-Phenylenebis(oxy)]dianiline;1,3-Phenylenebis(3-oxyaniline);SCHEMBL84301;Acetic acid, p-arsonophenoxy-;DTXSID4065109;AMY8630;1,3'-Bis(3-aminophenoxy)benzene;AKOS015895836;SB66376;AS-14991;SY033981;3-[3-(3-Aminophenoxy)phenoxy]phenylamine #;B1370;CS-0156879;FT-0606560;A801181;W-108791

Chemical Property of 1,3-Bis(3-aminophenoxy)benzene

Chemical Property:

• Vapor Pressure: 2.27E-09mmHg at 25°C
• Melting Point: 108 °C
• Refractive Index: 1.667
• Boiling Point: 479.9 °C at 760 mmHg
• PKA: 4.29±0.10(Predicted)
• Flash Point: 264.8 °C
• PSA: 70.50000
• Density: 1.243 g/cm³
• LogP: 5.59800
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature
• Water Solubility.: Insoluble in water
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 292.121177757
• Heavy Atom Count: 22
• Complexity: 309

Purity/Quality:

99% ^*data from raw suppliers

1,3-Bis(3-Aminophenoxy)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s): 20/21/22:
• Hazard Codes: 20/21/22:
• Statements: 20/21/22
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)OC2=CC(=CC=C2)OC3=CC=CC(=C3)N)N
• Uses: 1,3-BIS(3-AMINOPHENOXY)BENZENE is a useful research chemical.

Technology Process of 1,3-Bis(3-aminophenoxy)benzene

There total 3 articles about 1,3-Bis(3-aminophenoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1,3-bis(3-nitrophenoxy)benzene (54060-31-0) → 1,3-bis (3-aminophenoxy)-benzene (10526-07-5)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In ethanol; for 8h; under 15001.5 Torr;

Reference yield:

1,3-dibromobenzene (108-36-1) + m-Hydroxyaniline (591-27-5) → 1,3-bis (3-aminophenoxy)-benzene (10526-07-5)

Guidance literature:

With potassium hydroxide; copper; at 200 - 280 ℃;

Reference yield:

→ 1,3-bis (3-aminophenoxy)-benzene (10526-07-5)

Guidance literature:

upstream raw materials:

1,3-dibromobenzene

m-Hydroxyaniline

1,3-bis(3-nitrophenoxy)benzene

Downstream raw materials:

1,3-Dicyclohexylurea

Refernces

• 1、 -. "METHOD FOR PREPARING A POLY(ETHER SULFONIMIDE OR -AMIDE) COPOLYMER USING CYCLIC OLIGOMERS". . . Retrieved 2013/03/26.
• 2、 -. "Process for producing 1,3-bis (3-aminophenoxy) benzene". . . Retrieved 2008/06/13.